Document Detail


A rapid method for detection of N-acetylglucosaminidase-type chitinase activity in crossed immunoelectrophoresis and sodium dodecyl sulfate-polyacrylamide gel electrophoresis gels using 4-methylumbelliferyl-N-acetyl-D-glucosaminide as substrate.
MedLine Citation:
PMID:  7925246     Owner:  NLM     Status:  MEDLINE    
Abstract/OtherAbstract:
A method for the detection of N-acetylglucosaminidase (GlcNAcase) activity has been developed by using 4-methyl-umbelliferyl-N-acetyl-D-glucosaminide (4-MU-GlcNAc) as substrate in crossed immunoelectrophoresis (CIE) and sodium dodecyl sulfate-polyacrylamide gel electrophoresis (SDS-PAGE) gels. Visualization of the reaction with a 366 nm ultra-violet light is possible in approximately 30 min. The method is fast and sensitive in comparison with previous methods. The same band as in SDS-PAGE, showing both GlcNAcase and chitinase activity, was found in the present study; we therefore conclude that this method is also useful in a GlcNAcase-type chitinase assay.
Authors:
K S Chen; K K Lee; H C Chen
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Publication Detail:
Type:  Comparative Study; Journal Article; Research Support, Non-U.S. Gov't    
Journal Detail:
Title:  Electrophoresis     Volume:  15     ISSN:  0173-0835     ISO Abbreviation:  Electrophoresis     Publication Date:  1994 May 
Date Detail:
Created Date:  1994-10-26     Completed Date:  1994-10-26     Revised Date:  2007-11-15    
Medline Journal Info:
Nlm Unique ID:  8204476     Medline TA:  Electrophoresis     Country:  GERMANY    
Other Details:
Languages:  eng     Pagination:  662-5     Citation Subset:  IM    
Affiliation:
Department of Marine Food Science, National Taiwan Ocean University, Keelung, Republic of China.
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MeSH Terms
Descriptor/Qualifier:
Acetylglucosamine / analogs & derivatives*
Acetylglucosaminidase / analysis*
Chitinase / analysis*
Electrophoresis, Polyacrylamide Gel / instrumentation*
Fluorescence
Gels*
Hymecromone / analogs & derivatives*
Immunoelectrophoresis, Two-Dimensional / instrumentation*
Sensitivity and Specificity
Substrate Specificity
Time Factors
Chemical
Reg. No./Substance:
0/Gels; 37067-30-4/4-methylumbelliferyl 2-acetamido-2-deoxy-beta-D-glucopyranoside; 7512-17-6/Acetylglucosamine; 90-33-5/Hymecromone; EC 3.2.1.14/Chitinase; EC 3.2.1.52/Acetylglucosaminidase

From MEDLINE®/PubMed®, a database of the U.S. National Library of Medicine


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