Document Detail


A quantitative nitroblue tetrazolium assay for determining intracellular superoxide anion production in phagocytic cells.
MedLine Citation:
PMID:  16450867     Owner:  NLM     Status:  MEDLINE    
Abstract/OtherAbstract:
Conventionally, a semi-quantitative microscopic nitroblue tetrazolium (NBT) assay is used to determine the production of superoxide anion (O2(-)) in various phagocytic cells. This microscopic assay is conducted by counting the cells containing blue NBT formazan deposits, which are formed by reduction of the membrane permeable, water-soluble, yellow-colored, nitroblue tetrazolium (Y-NBT) by O2(-). However, this assay is semi-quantitative and is prone to observer bias. In the present study, we modified the NBT assay by dissolving the blue formazan particles using 2M potassium hydroxide and dimethylsulfoxide and then measured its absorbance using a microplate reader at 620nm. The absorbance of dissolved NBT increased in proportion to cell number (r = 0.9907), incubation time, and stimulus concentration. To test the usefulness of this modified assay, we compared the abilities of a number of types of phagocytic cells to produce O2(-). The cells examined included murine macrophage cell lines (RAW 264.7 and J774), freshly prepared murine peritoneal macrophages and neutrophils, a human myeloid cell line (PLB-985), and freshly prepared human peripheral blood neutrophils. In addition, we demonstrate that nitric oxide produced by RAW 264.7 cells does not interfere with the modified colorimetric NBT assay. Taken together, our results indicate that the modified colorimetric NBT assay is simple, sensitive, and quantitative, and that it can be used to determine the amounts of intracellular O2(-) produced by phagocytic cells. Thus, this assay is sensitive enough to measure, quantitatively, even the small amounts of O2(-) produced in monocytes and macrophages that are not detectable by the conventional microscopic NBT assay.
Authors:
Hyung Sim Choi; Jun Woo Kim; Young-Nam Cha; Chaekyun Kim
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Publication Detail:
Type:  Comparative Study; Journal Article; Research Support, Non-U.S. Gov't    
Journal Detail:
Title:  Journal of immunoassay & immunochemistry     Volume:  27     ISSN:  1532-1819     ISO Abbreviation:  J Immunoassay Immunochem     Publication Date:  2006  
Date Detail:
Created Date:  2006-02-02     Completed Date:  2006-03-15     Revised Date:  2006-11-15    
Medline Journal Info:
Nlm Unique ID:  100963688     Medline TA:  J Immunoassay Immunochem     Country:  United States    
Other Details:
Languages:  eng     Pagination:  31-44     Citation Subset:  IM    
Affiliation:
Laboratory of Cell Signaling, Inha University College of Medicine, Incheon, Korea.
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MeSH Terms
Descriptor/Qualifier:
Animals
Biological Assay / methods
Cell Line
Cells, Cultured
Cytochromes c / metabolism
Dimethyl Sulfoxide
Humans
Hydroxides
Macrophages / metabolism*
Mice
Mice, Inbred C57BL
Neutrophils / metabolism*
Nitric Oxide / metabolism
Nitroblue Tetrazolium / metabolism*
Oxidation-Reduction
Potassium Compounds
Superoxide Dismutase / antagonists & inhibitors
Superoxides / metabolism*
Chemical
Reg. No./Substance:
0/Hydroxides; 0/Potassium Compounds; 10102-43-9/Nitric Oxide; 11062-77-4/Superoxides; 1310-58-3/potassium hydroxide; 298-83-9/Nitroblue Tetrazolium; 67-68-5/Dimethyl Sulfoxide; 9007-43-6/Cytochromes c; EC 1.15.1.1/Superoxide Dismutase

From MEDLINE®/PubMed®, a database of the U.S. National Library of Medicine


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