| A new method for the protection of carboxylic acids with a triisopropylsiloxymethyl group. | |
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MedLine Citation:
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PMID: 23036974 Owner: NLM Status: In-Data-Review |
Abstract/OtherAbstract:
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An effective method for the protection of carboxylic acids with a triisopropylsiloxymethyl (TIPSOCH(2)) group is described. The reactions of various carboxylic acids with C(12)H(25)SCH(2)OTIPS in the presence of CuBr(2), Et(3)N, and molecular sieves 4A afford the corresponding triisopropylsiloxymethyl esters in good yields. |
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Authors:
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Hikaru Yoshimura; Kohei Eto; Keisuke Takahashi; Jun Ishihara; Susumi Hatakeyama |
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Publication Detail:
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Type: Journal Article |
Journal Detail:
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Title: Chemical & pharmaceutical bulletin Volume: 60 ISSN: 1347-5223 ISO Abbreviation: Chem. Pharm. Bull. Publication Date: 2012 |
Date Detail:
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Created Date: 2012-10-05 Completed Date: - Revised Date: - |
Medline Journal Info:
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Nlm Unique ID: 0377775 Medline TA: Chem Pharm Bull (Tokyo) Country: Japan |
Other Details:
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Languages: eng Pagination: 1334-9 Citation Subset: IM |
Affiliation:
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Graduate School of Biomedical Sciences, Nagasaki University. |
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From MEDLINE®/PubMed®, a database of the U.S. National Library of Medicine
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