Document Detail


A new approach for extension of the identification period of irradiated cellulose-containing foodstuffs by EPR spectroscopy.
MedLine Citation:
PMID:  10697727     Owner:  NLM     Status:  MEDLINE    
Abstract/OtherAbstract:
We report on the possibility of identification by EPR spectroscopy of some irradiated cellulose-containing foodstuffs, at a relatively long time after the irradiation, when the characteristic EPR spectral lines of the cellulose free radical have essentially disappeared. In such cases rather expensive and time-consuming methods (e.g. thermoluminescence analysis) have to be applied. The present communication demonstrates with some pre-irradiated spices, dried medicinal and sweet herbs that simply heating the samples to 60 degrees C for one hour leads to a significant (50% or more) decrease of the EPR intensity of the remaining central line of the samples. For comparison, the loss in the intensity of the same line upon heating non-irradiated samples at 60 degrees C for one hour was only about 10%. This inexpensive new procedure will extend the post-irradiation period in which EPR can be used for distinguishing irradiated from non-irradiated samples, of certain cellulose-containing foodstuffs.
Authors:
N D Yordanov; V Gancheva
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Publication Detail:
Type:  Journal Article; Research Support, Non-U.S. Gov't    
Journal Detail:
Title:  Applied radiation and isotopes : including data, instrumentation and methods for use in agriculture, industry and medicine     Volume:  52     ISSN:  0969-8043     ISO Abbreviation:  Appl Radiat Isot     Publication Date:  2000 Feb 
Date Detail:
Created Date:  2000-03-31     Completed Date:  2000-03-31     Revised Date:  2008-11-21    
Medline Journal Info:
Nlm Unique ID:  9306253     Medline TA:  Appl Radiat Isot     Country:  ENGLAND    
Other Details:
Languages:  eng     Pagination:  195-8     Citation Subset:  IM    
Affiliation:
Institute of Catalysis, Bulgarian Academy of Sciences, Sofia, Bulgaria. ndyepr@bas.bg
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MeSH Terms
Descriptor/Qualifier:
Angiosperms
Cellulose / analysis*
Electron Spin Resonance Spectroscopy / methods
Food Analysis / methods*
Food Irradiation*
Hot Temperature
Plants, Medicinal
Spices
Chemical
Reg. No./Substance:
9004-34-6/Cellulose

From MEDLINE®/PubMed®, a database of the U.S. National Library of Medicine


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