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A method for fast analysis of volatile components of Citrus aurantium L. leaves.
MedLine Citation:
PMID:  23039826     Owner:  NLM     Status:  Publisher    
Abstract/OtherAbstract:
To avoid the traditional and time consuming hydrodistillation, the analyses of volatile components in leaves of Citrus aurantium L. were carried out by a simple microwave distillation followed by headspace single drop microextraction (MD-HS-SDME) coupled to gas chromatography-mass spectrometry (GC-MS). The headspace volatile compounds were collected after irradiation using a single drop of n-heptadecan. The extraction conditions were optimized using the relative peak areas as index. The chemical composition of the MD-HS-SDME extracts was confirmed according to their retention indexes and mass spectra. Forty-one components were extracted and identified by using the MD-HS-SDME method. Limonene (62%), Linalool (7.47%), trans-β-Ocimene (3.47%), Caryophyllene (2.05%), α- Bisabolene (1.8%) and Myrcene (1.18%) were the major constituents.
Authors:
Mohammad Bagher Gholivand; Marzieh Piryaei
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Publication Detail:
Type:  JOURNAL ARTICLE     Date:  2012-10-5
Journal Detail:
Title:  Natural product research     Volume:  -     ISSN:  1478-6427     ISO Abbreviation:  Nat. Prod. Res.     Publication Date:  2012 Oct 
Date Detail:
Created Date:  2012-10-8     Completed Date:  -     Revised Date:  -    
Medline Journal Info:
Nlm Unique ID:  101167924     Medline TA:  Nat Prod Res     Country:  -    
Other Details:
Languages:  ENG     Pagination:  -     Citation Subset:  -    
Affiliation:
a Faculty of Chemistry, Department of Analytical Chemistry , Razi University , Kermanshah , Iran.
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