Document Detail


A high performance liquid chromatographic procedure for the simultaneous determination of norfloxacin and furprofen in rat plasma.
MedLine Citation:
PMID:  8318826     Owner:  NLM     Status:  MEDLINE    
Abstract/OtherAbstract:
A rapid and simple high performance liquid chromatographic analytical method is described for the simultaneous determination of norfloxacin and furprofen in rat plasma. Following dichloromethane extraction, the solution was chromatographed in a Vydac anion exchange column using a mobile phase of 0.05 M phosphate buffer (pH = 7.0): acetonitrile (80:20, v/v) at a flow-rate of 1.8 mL/min. The drugs were detected by UV absorption at 278 nm. The total chromatographic analysis time was 10 min. The response was linear, 0.1-5.0 micrograms/mL for norfloxacin and 0.1-3.0 micrograms/mL for furprofen, respectively. This method is useful for pharmacokinetic studies of these compounds and will facilitate detailed investigations into the interactions between quinolones and furprofen.
Authors:
G Carlucci; P Mazzeo; G Palumbo
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Publication Detail:
Type:  Journal Article; Research Support, Non-U.S. Gov't    
Journal Detail:
Title:  Biomedical chromatography : BMC     Volume:  7     ISSN:  0269-3879     ISO Abbreviation:  Biomed. Chromatogr.     Publication Date:    1993 May-Jun
Date Detail:
Created Date:  1993-07-30     Completed Date:  1993-07-30     Revised Date:  2006-11-15    
Medline Journal Info:
Nlm Unique ID:  8610241     Medline TA:  Biomed Chromatogr     Country:  ENGLAND    
Other Details:
Languages:  eng     Pagination:  126-8     Citation Subset:  IM    
Affiliation:
Dipartimento di Chimica, Ingegneria Chimica e Materiali, Università dell'Aquila, Italy.
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MeSH Terms
Descriptor/Qualifier:
Animals
Chromatography, High Pressure Liquid / methods*,  standards,  statistics & numerical data
Female
Male
Norfloxacin / blood*
Phenylpropionates / blood*
Quality Control
Rats
Rats, Sprague-Dawley
Chemical
Reg. No./Substance:
0/Phenylpropionates; 66318-17-0/furprofen; 70458-96-7/Norfloxacin

From MEDLINE®/PubMed®, a database of the U.S. National Library of Medicine


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