Document Detail


A handy detection cell for end-column electrochemical detection in capillary electrophoresis.
MedLine Citation:
PMID:  11783786     Owner:  NLM     Status:  PubMed-not-MEDLINE    
Abstract/OtherAbstract:
A handy and simple detection cell was constructed using a mixing joint for end-column electrochemical detection in capillary electrophoresis (CE). The cell allows for positioning of the working electrode at the end of the separation capillary without the aid of micropositioners. The design facilitates the exchange of electrodes and capillaries without the need to refabricate the entire capillary-electrode setup. The cell can be assembled in a short period of time. Alignment with the joint screw proved to be reproducible for working electrodes of copper and gold. The advantages of reduced time and low cost make the device very attractive for the routine analysis of electroactive species, such as carbohydrates and their derivatives, purine bases and nucleosides, amino acids, and catecholamines etc. by CE with electrochemical detection.
Authors:
M Goto; S Inagaki; Y Esaka
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Publication Detail:
Type:  Journal Article    
Journal Detail:
Title:  Analytical sciences : the international journal of the Japan Society for Analytical Chemistry     Volume:  17     ISSN:  0910-6340     ISO Abbreviation:  Anal Sci     Publication Date:  2001 Dec 
Date Detail:
Created Date:  2002-01-09     Completed Date:  2002-02-14     Revised Date:  2003-10-31    
Medline Journal Info:
Nlm Unique ID:  8511078     Medline TA:  Anal Sci     Country:  Japan    
Other Details:
Languages:  eng     Pagination:  1383-7     Citation Subset:  -    
Affiliation:
Department of Pharmaceutical Analytical Chemistry, Gifu Pharmaceutical University, Japan.
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