| A convenient synthesis of 3 beta,12 alpha-, 3 beta,7 alpha-, and 3 beta,7 beta-dihydroxy-5-cholen-24-oic acids: unusual bile acids in human biological fluids. | |
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MedLine Citation:
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PMID: 3445285 Owner: NLM Status: MEDLINE |
Abstract/OtherAbstract:
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The unusual bile acids 3 beta,12 alpha- (V), 3 beta,7 alpha- (XIIIa), and 3 beta,7 beta- (XIIIb) dihydroxy-5-cholen-24-oic acids were synthesized conveniently from the 3-oxo derivatives of deoxycholic (I) and lithocholic (VI) acids, respectively, to provide authentic samples for the gas chromatography-mass spectrometric determination of these bile acids in the abnormal metabolism of bile acids. |
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Authors:
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M Tohma; R Mahara; H Takeshita; T Kurosawa |
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Publication Detail:
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Type: Journal Article |
Journal Detail:
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Title: Steroids Volume: 48 ISSN: 0039-128X ISO Abbreviation: Steroids Publication Date: 1986 Nov-Dec |
Date Detail:
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Created Date: 1988-04-25 Completed Date: 1988-04-25 Revised Date: 2006-11-15 |
Medline Journal Info:
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Nlm Unique ID: 0404536 Medline TA: Steroids Country: UNITED STATES |
Other Details:
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Languages: eng Pagination: 331-8 Citation Subset: IM |
Affiliation:
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Faculty of Pharmaceutical Sciences, Higashi-Nippon-Gakuen University, Hokkaido, Japan. |
Export Citation:
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APA/MLA Format Download EndNote Download BibTex |
| MeSH Terms | |
Descriptor/Qualifier:
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Bile Acids and Salts
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analysis* Body Fluids / analysis* Chenodeoxycholic Acid / analogs & derivatives*, analysis Cholic Acids / analysis* Gas Chromatography-Mass Spectrometry Humans Magnetic Resonance Spectroscopy |
| Chemical | |
Reg. No./Substance:
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0/Bile Acids and Salts; 0/Cholic Acids; 19246-13-0/3,7-dihydroxychol-5-enoic acid; 474-25-9/Chenodeoxycholic Acid; 63266-92-2/3,12-dihydroxy-5-cholenoic acid |
From MEDLINE®/PubMed®, a database of the U.S. National Library of Medicine
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