Document Detail


Uronic acid determination by high performance liquid chromatography with postcolumn fluorescence derivatization.
MedLine Citation:
PMID:  16956616     Owner:  NLM     Status:  MEDLINE    
Abstract/OtherAbstract:
To develop a fluorimetric high performance liquid chromatography (HPLC) technique for uronic acid microanalysis, a saline mobile phase and the postcolumn fluorimetric determination were combined. The detection limits of D-glucuronic, D-galacturonic and D-mannuronic acids were 7.19, 23.88 and 7.08 pmol, respectively. The proposed method was successfully applied to uronic acid microanalysis in a polysaccharide hydrolysate and a drink.
Authors:
Hirotaka Kakita; Hiroshi Kamishima; Kuniyo Inouye
Related Documents :
17638346 - Preparation of a new chiral stationary phase for hplc based on the (r)- 1-phenyl-2-(4-m...
11043786 - Configurational analysis of chiral acids as o-trifluoroacetylated (-)-menthyl esters by...
8590926 - Determination of monoamine oxidase b activity by high-performance liquid chromatography...
16239006 - Simple method for the separation and detection of native amino acids and the identifica...
4562406 - Effect of ph on adenine and amino acid uptake during sporulation in saccharomyces cerev...
11576826 - Evaluation of skin sensitization potential of melatonin and nimesulide by murine local ...
Publication Detail:
Type:  Journal Article     Date:  2006-09-07
Journal Detail:
Title:  Journal of chromatography. A     Volume:  1129     ISSN:  0021-9673     ISO Abbreviation:  J Chromatogr A     Publication Date:  2006 Oct 
Date Detail:
Created Date:  2006-09-18     Completed Date:  2006-11-22     Revised Date:  2009-01-15    
Medline Journal Info:
Nlm Unique ID:  9318488     Medline TA:  J Chromatogr A     Country:  Netherlands    
Other Details:
Languages:  eng     Pagination:  296-9     Citation Subset:  IM    
Affiliation:
AIST Shikoku, National Institute of Advanced Industrial Science and Technology (AIST), Takamatsu, Kagawa, Japan. h-kakita@aist.go.jp
Export Citation:
APA/MLA Format     Download EndNote     Download BibTex
MeSH Terms
Descriptor/Qualifier:
Chromatography, High Pressure Liquid / instrumentation,  methods*
Fluorescence
Glucose / analysis,  chemistry
Glucuronates / analysis,  chemistry
Hexuronic Acids / analysis,  chemistry
Reproducibility of Results
Uronic Acids / analysis*,  chemistry
Chemical
Reg. No./Substance:
0/Glucuronates; 0/Hexuronic Acids; 0/Uronic Acids; 14982-50-4/galacturonic acid; 50-99-7/Glucose; 6814-36-4/mannuronic acid

From MEDLINE®/PubMed®, a database of the U.S. National Library of Medicine


Previous Document:  Reversed-phase liquid chromatograhy/electrospray ionization tandem mass spectrometry for analysis of...
Next Document:  Application of gas chromatography-hybrid chemical ionization mass spectrometry to the analysis of di...