Document Detail


Truncated cystatin C in cerebrospiral fluid: Technical [corrected] artefact or biological process?
MedLine Citation:
PMID:  16021609     Owner:  NLM     Status:  MEDLINE    
Abstract/OtherAbstract:
Cystatin C, a low molecular weight cysteine proteinase inhibitor present in human body fluids at physiological concentrations, is more expressed in cerebrospinal fluid (CSF) than in plasma. Mass spectrometric characterization showed that after 3 months of storage of human CSF at -20 degrees C, cystatin C was cleaved in the peptide bond between R8 and L9 and lost its eight N-termini amino acids, whereas this cleavage did not occur when stored at -80 degrees C. This truncation occurred in all CSF samples studied irrespective of the underlying neurological status, indicating a storage-related artefact rather than a physiological or pathological processing of the protein. These results stress the importance of optimal preanalytical storage conditions of any sample prior to proteomics studies.
Authors:
Odile Carrette; Pierre R Burkhard; Severine Hughes; Denis F Hochstrasser; Jean-Charles Sanchez
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Publication Detail:
Type:  Journal Article    
Journal Detail:
Title:  Proteomics     Volume:  5     ISSN:  1615-9853     ISO Abbreviation:  Proteomics     Publication Date:  2005 Aug 
Date Detail:
Created Date:  2005-08-10     Completed Date:  2005-10-11     Revised Date:  2008-11-21    
Medline Journal Info:
Nlm Unique ID:  101092707     Medline TA:  Proteomics     Country:  Germany    
Other Details:
Languages:  eng     Pagination:  3060-5     Citation Subset:  IM    
Affiliation:
Biomedical Proteomics Research Group, Geneva University Hospital and Medical School, 1 rue Michel Servet, CH-1211 Geneva 4, Switzerland. Odile.Carrette@medecine.unige.ch
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MeSH Terms
Descriptor/Qualifier:
Artifacts
Cystatin C
Cystatins / cerebrospinal fluid*,  chemistry*
Cysteine Proteinase Inhibitors / chemistry
Electrophoresis, Polyacrylamide Gel
Humans
Mass Spectrometry / methods
Protein Array Analysis
Protein Structure, Tertiary
Proteins / chemistry
Proteomics / methods
Specimen Handling
Spectrometry, Mass, Matrix-Assisted Laser Desorption-Ionization
Temperature
Time Factors
Chemical
Reg. No./Substance:
0/CST3 protein, human; 0/Cystatin C; 0/Cystatins; 0/Cysteine Proteinase Inhibitors; 0/Proteins
Comments/Corrections
Erratum In:
Proteomics. 2005 Sep;5(14):3822

From MEDLINE®/PubMed®, a database of the U.S. National Library of Medicine


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