Document Detail


Theoretical analysis of a site-specific chemiluminescence reaction and its application to quantitation of lipid hydroperoxides.
MedLine Citation:
PMID:  3242948     Owner:  NLM     Status:  MEDLINE    
Abstract/OtherAbstract:
A system was designed for chemiluminescent measurement of lipid hydroperoxides by their site-specific reaction in sodium dodecylsulfate micelles. Ferrous ion-induced decomposition of lipid hydroperoxides in the sodium dodecylsulfate micelles resulted in strong chemiluminescence of the Cypridina luciferin analog, 2-methyl-6-phenyl-3,7-dihydroimidazo[1,2-alpha]pyrazin-3-one (CLA). After addition of ferrous sulfate to the micelles containing lipid hydroperoxide and luciferin, the chemiluminescence intensity reached a maximum rapidly and then decreased. The sequence of this reaction was elucidated by theoretical analysis, which demonstrated that the maximum chemiluminescence intensity is proportional to the initial concentration of hydroperoxide. Good linear relationships were observed between the maximum counts of chemiluminescence and the amounts of hydroperoxides of linoleic acid, phosphatidylcholine, choresterol (5 alpha), cumene and tert-butyl and hydrogen peroxide. This chemiluminescence method was simple and sensitive enough to detect picomole levels of linoleic acid and phosphatidylcholine hydroperoxides.
Authors:
K Fukuzawa; T Yoshimura; T Fujii; K Takauchi; M Miki; H Tamai; M Mino
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Publication Detail:
Type:  Journal Article    
Journal Detail:
Title:  Chemistry and physics of lipids     Volume:  48     ISSN:  0009-3084     ISO Abbreviation:  Chem. Phys. Lipids     Publication Date:  1988 Oct 
Date Detail:
Created Date:  1989-05-26     Completed Date:  1989-05-26     Revised Date:  2006-11-15    
Medline Journal Info:
Nlm Unique ID:  0067206     Medline TA:  Chem Phys Lipids     Country:  NETHERLANDS    
Other Details:
Languages:  eng     Pagination:  197-203     Citation Subset:  IM    
Affiliation:
Faculty of Pharmaceutical Sciences, University of Tokushima, Japan.
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MeSH Terms
Descriptor/Qualifier:
Binding Sites
Ferrous Compounds / metabolism
Lipid Peroxides / analysis*
Luminescent Measurements*
Micelles
Oxidation-Reduction
Chemical
Reg. No./Substance:
0/Ferrous Compounds; 0/Lipid Peroxides; 0/Micelles

From MEDLINE®/PubMed®, a database of the U.S. National Library of Medicine


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