Document Detail

Synthesis of macrocycle isomers via metathesis cyclization and their self-assembly from aqueous solutions.
MedLine Citation:
PMID:  18808129     Owner:  NLM     Status:  PubMed-not-MEDLINE    
Novel triangular macrocycle isomers were synthesized through metathesis cyclization with high yield (77%). HPLC and MALDI-TOF showed that the purity of the macrocycles was higher than 99%, while (1)H NMR clearly showed that these macrocycles contain C2 and C3 isomers in a ratio of 1:3. AFM and TEM showed that they spontaneously formed vesicular structures in a chloroform/water system with an average diameter of 460 nm, which was corroborated by DLS results.
Jing Jiang; Gregory N Tew
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Publication Detail:
Type:  Journal Article     Date:  2008-09-23
Journal Detail:
Title:  Organic letters     Volume:  10     ISSN:  1523-7052     ISO Abbreviation:  Org. Lett.     Publication Date:  2008 Oct 
Date Detail:
Created Date:  2008-10-09     Completed Date:  2008-12-10     Revised Date:  -    
Medline Journal Info:
Nlm Unique ID:  100890393     Medline TA:  Org Lett     Country:  United States    
Other Details:
Languages:  eng     Pagination:  4393-6     Citation Subset:  -    
Department of Polymer Science and Engineering, University of Massachusetts, Amherst, Massachusetts 01003, USA.
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