Document Detail


Synthesis and characterization of thiomers of polyaspartamide type.
MedLine Citation:
PMID:  15707748     Owner:  NLM     Status:  MEDLINE    
Abstract/OtherAbstract:
Synthesis of poly[alpha,beta-(N-2-hydroxyethyl-DL-aspartamide)]-thioglycolic acid (PHEA-TGA) conjugate as a new polyaspartamide thiomer is described. The parent polymer PHEA is chemically modified by introducing sulphydryl-bearing compound thioglycolic acid. By varying the reaction conditions several batches of PHEA-TGA conjugates were prepared and analyzed. Tensile studies revealed that total work of adhesion of PHEA-TGA increased more than twice compared to the unmodified polymer. Microparticles prepared from the thiolated polymer preserved its bioadhesive properties.
Authors:
M Bubenik Bilicić; J Filipović-Grcić; A Martinac; M Barbarić; B Zorc; B Cetina-Cizmek; P Tudja
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Publication Detail:
Type:  Journal Article; Research Support, Non-U.S. Gov't     Date:  2004-12-29
Journal Detail:
Title:  International journal of pharmaceutics     Volume:  291     ISSN:  0378-5173     ISO Abbreviation:  Int J Pharm     Publication Date:  2005 Mar 
Date Detail:
Created Date:  2005-02-14     Completed Date:  2006-04-21     Revised Date:  2006-11-15    
Medline Journal Info:
Nlm Unique ID:  7804127     Medline TA:  Int J Pharm     Country:  Netherlands    
Other Details:
Languages:  eng     Pagination:  211-9     Citation Subset:  IM    
Affiliation:
PLIVA-Research Institute, Ltd., Prilaz Baruna Filipovića 29, 10000 Zagreb, Croatia.
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MeSH Terms
Descriptor/Qualifier:
Chemistry, Pharmaceutical / methods
Particle Size
Peptides / analysis,  chemical synthesis*
Polymers / analysis,  chemical synthesis*
Spectroscopy, Near-Infrared / methods
Technology, Pharmaceutical / methods
Thioglycolates / analysis,  chemical synthesis*
Chemical
Reg. No./Substance:
0/Peptides; 0/Polymers; 0/Thioglycolates; 0/alpha,beta-poly((2-hydroxyethyl)-aspartamide)

From MEDLINE®/PubMed®, a database of the U.S. National Library of Medicine


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