Document Detail


Synthesis and biophysical studies on fluorescently labeled oligodeoxyribonucleotides.
MedLine Citation:
PMID:  17578747     Owner:  NLM     Status:  MEDLINE    
Abstract/OtherAbstract:
Two highly fluorescent compounds, viz. 6-(6-isobutyrylamino-1,3-dioxo-1 H,3H-benzo[de]isoquinolin-2-yl)-hexanoic acid and 6-(6-dimethylamino-1,3-dioxo-1 H,3H-benzo[de]isoqu-inolin-2-yl)-hexanoic acid have been synthesized, characterized, and attached to 12-mer oligodeoxyribonucleotides at their 5'-end using suitable linker molecule. These labeled oligodeoxyribonucleotides have shown appreciable fluorescence even at 0.0019 microM concentrations. Thermal denaturation studies have shown comparatively higher Tm values when oligodeoxyribonucleotides are labeled. These labeled oligodeoxyribonucleotides have been purified on RP-HPLC utilizing their hydrophobicity and on polyacrylamide gel because of their easy detection due to fluorescence.
Authors:
Shipra Singh; Pradeep Kumar; K C Gupta; Ramendra K Singh
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Publication Detail:
Type:  Journal Article    
Journal Detail:
Title:  Nucleosides, nucleotides & nucleic acids     Volume:  26     ISSN:  1525-7770     ISO Abbreviation:  Nucleosides Nucleotides Nucleic Acids     Publication Date:  2007  
Date Detail:
Created Date:  2007-06-20     Completed Date:  2007-10-01     Revised Date:  -    
Medline Journal Info:
Nlm Unique ID:  100892832     Medline TA:  Nucleosides Nucleotides Nucleic Acids     Country:  United States    
Other Details:
Languages:  eng     Pagination:  521-31     Citation Subset:  IM    
Affiliation:
Nucleic Acids Research Laboratory, Department of Chemistry, University of Allahabad, Allahabad, India.
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MeSH Terms
Descriptor/Qualifier:
Chromatography, High Pressure Liquid
Electrophoresis, Polyacrylamide Gel
Fluorescence*
Hexanoic Acids / chemical synthesis,  chemistry
Isoquinolines / chemical synthesis,  chemistry
Oligodeoxyribonucleotides / chemical synthesis*,  chemistry*
Spectrometry, Fluorescence
Spectrophotometry, Ultraviolet
Transition Temperature
Chemical
Reg. No./Substance:
0/6-(6-dimethylamino-1,3-dioxo-1H,3H-benzo(de)isoquinolin-2-yl)hexanoic acid; 0/6-(6-isobutyrylamino-1,3-dioxo-1H,3H-benzo(de)isoquinolin-2-yl)hexanoic acid; 0/Hexanoic Acids; 0/Isoquinolines; 0/Oligodeoxyribonucleotides

From MEDLINE®/PubMed®, a database of the U.S. National Library of Medicine


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