Document Detail


Structural and functional basis of resistance to neuraminidase inhibitors of influenza B viruses.
MedLine Citation:
PMID:  20695427     Owner:  NLM     Status:  MEDLINE    
Abstract/OtherAbstract:
We have identified a virus, B/Perth/211/2001, with a spontaneous mutation, D197E in the neuraminidase (NA), which confers cross-resistance to all NA inhibitors. We analyzed enzyme properties of the D197 and E197 NAs and compared these to a D197N NA, known to arise after oseltamivir treatment. Zanamivir and peramivir bound slowly to the wild type NA, but binding of oseltamivir was more rapid. The D197E/N mutations resulted in faster binding of all three inhibitors. Analysis of the crystal structures of D197 and E197 NAs with and without inhibitors showed that the D197E mutation compromised the interaction of neighboring R150 with the N-acetyl group, common to the substrate sialic acid and all NA inhibitors. Although rotation of the E275 in the NA active site occurs upon binding peramivir in both the D197 and E197 NAs, this does not occur upon binding oseltamivir in the E197 NA. Lack of the E275 rotation would also account for the loss of slow binding and the partial resistance of influenza B wild type NAs to oseltamivir.
Authors:
Aaron J Oakley; Susan Barrett; Thomas S Peat; Janet Newman; Victor A Streltsov; Lynne Waddington; Takehiko Saito; Masato Tashiro; Jennifer L McKimm-Breschkin
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Publication Detail:
Type:  Journal Article; Research Support, N.I.H., Extramural; Research Support, Non-U.S. Gov't    
Journal Detail:
Title:  Journal of medicinal chemistry     Volume:  53     ISSN:  1520-4804     ISO Abbreviation:  J. Med. Chem.     Publication Date:  2010 Sep 
Date Detail:
Created Date:  2010-09-02     Completed Date:  2010-09-30     Revised Date:  -    
Medline Journal Info:
Nlm Unique ID:  9716531     Medline TA:  J Med Chem     Country:  United States    
Other Details:
Languages:  eng     Pagination:  6421-31     Citation Subset:  IM    
Affiliation:
CSIRO Materials Science and Engineering, Parkville, 343 Royal Parade, Parkville, Victoria, 3052, Australia.
Data Bank Information
Bank Name/Acc. No.:
PDB/3K36;  3K37;  3K38;  3K39;  3K3A
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MeSH Terms
Descriptor/Qualifier:
Antiviral Agents / chemistry*
Crystallography, X-Ray
Cyclopentanes / chemistry*
Drug Resistance, Viral*
Guanidines / chemistry*
Hydrogen Bonding
Influenza B virus / enzymology*
Models, Molecular
Molecular Structure
Mutation
Neuraminidase / antagonists & inhibitors*,  chemistry*,  genetics
Oseltamivir / chemistry*
Protein Binding
Zanamivir / chemistry*
Grant Support
ID/Acronym/Agency:
R01A1062721//PHS HHS
Chemical
Reg. No./Substance:
0/Antiviral Agents; 0/Cyclopentanes; 0/Guanidines; 0/Oseltamivir; 0/peramivir; 139110-80-8/Zanamivir; EC 3.2.1.18/Neuraminidase

From MEDLINE®/PubMed®, a database of the U.S. National Library of Medicine


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