| Simultaneous determination of 11 characteristic components in three species of Curcuma rhizomes using pressurized liquid extraction and high-performance liquid chromatography. | |
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MedLine Citation:
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PMID: 17018231 Owner: NLM Status: MEDLINE |
Abstract/OtherAbstract:
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A high-performance liquid chromatography coupled with diode array detection (HPLC-DAD) and pressurized liquid extraction was developed for simultaneous quantitative determination of 11 characteristic compounds, including curcumenone, curcumenol, neocurdione, curdione, isocurcumenol, furanodienone, curcumol, germacrone, curzerene, furanodiene and beta-elemene, in rhizomes of three species of Curcuma. The analysis was performed on an ODS C18 column. The mobile phase consisted of (A) water and (B) acetonitrile using a gradient elution. The peaks were monitored at both 214 nm and 256 nm. All calibration curves showed good linearity (r2 > 0.9996) within test ranges. This method showed good repeatability for the quantification of these eleven components in three species Curcuma rhizomes with intra- and inter-day variations of less than 1.57% and 1.98%, respectively. The validated method was successfully applied to quantify 11 investigated components in eighteen samples of three species of Curcuma, which is helpful to control their quality. |
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Authors:
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F Q Yang; Y T Wang; S P Li |
Publication Detail:
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Type: Journal Article; Research Support, Non-U.S. Gov't Date: 2006-10-02 |
Journal Detail:
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Title: Journal of chromatography. A Volume: 1134 ISSN: 0021-9673 ISO Abbreviation: J Chromatogr A Publication Date: 2006 Nov |
Date Detail:
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Created Date: 2006-12-05 Completed Date: 2007-01-04 Revised Date: 2009-01-15 |
Medline Journal Info:
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Nlm Unique ID: 9318488 Medline TA: J Chromatogr A Country: Netherlands |
Other Details:
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Languages: eng Pagination: 226-31 Citation Subset: IM |
Affiliation:
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Institute of Chinese Medical Sciences, University of Macau, Macau, China. |
Export Citation:
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APA/MLA Format Download EndNote Download BibTex |
| MeSH Terms | |
Descriptor/Qualifier:
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Acetonitriles
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metabolism Calibration Chromatography, Gas Chromatography, High Pressure Liquid Curcuma / chemistry*, classification* Mass Spectrometry Plant Extracts / analysis*, chemistry, isolation & purification* Regression Analysis Rhizome / chemistry* |
| Chemical | |
Reg. No./Substance:
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0/Acetonitriles; 0/Plant Extracts |
From MEDLINE®/PubMed®, a database of the U.S. National Library of Medicine
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