Document Detail


Shortcut access to peptidosteroid conjugates: building blocks for solid-phase bile Acid scaffold decoration by convergent ligation.
MedLine Citation:
PMID:  22157580     Owner:  NLM     Status:  In-Data-Review    
Abstract/OtherAbstract:
We present three versatile solid-supported scaffold building blocks based on the (deoxy)cholic acid framework and decorated with handles for further derivatization by modern ligation techniques such as click chemistry, Staudinger ligation or native chemical ligation. Straightforward procedures are presented for the synthesis and analysis of the steroid constructs. These building blocks offer a new, facile and shorter access route to bile acid-peptide conjugates on solid-phase with emphasis on heterodipodal conjugates with defined spatial arrangements. As such, we provide versatile new synthons to the toolbox for bile acid decoration.
Authors:
Dieter Verzele; Sara Figaroli; Annemieke Madder
Publication Detail:
Type:  Journal Article     Date:  2011-12-07
Journal Detail:
Title:  Molecules (Basel, Switzerland)     Volume:  16     ISSN:  1420-3049     ISO Abbreviation:  Molecules     Publication Date:  2011  
Date Detail:
Created Date:  2011-12-14     Completed Date:  -     Revised Date:  -    
Medline Journal Info:
Nlm Unique ID:  100964009     Medline TA:  Molecules     Country:  Switzerland    
Other Details:
Languages:  eng     Pagination:  10168-86     Citation Subset:  IM    
Affiliation:
Laboratory for Organic and Biomimetic Chemistry, Department of Organic Chemistry, Faculty of Sciences, Ghent University, B-9000 Ghent, Belgium. annemieke.madder@ugent.be.
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