Document Detail


Short Synthesis of Alkyl-Substituted Acenes Using Carbonyl-Directed C-H and C-O Functionalization.
MedLine Citation:
PMID:  22794078     Owner:  NLM     Status:  Publisher    
Abstract/OtherAbstract:
A convenient method for the synthesis of tetraalkylanthracenes and -pentacenes by means of ruthenium-catalyzed regioselective C-H alkylation of the corresponding acenequinones was developed. Dialkyldiarylpentacene was also synthesized using chemoselective tandem C-H alkylation/C-O arylation of dimethoxypentacenequinone. It was suggested that a tetraalkylpentacene is stable under air in the dark and possesses an appropriate HOMO level as active material for p-type organic field-effect transistors (OFETs).
Authors:
Daiki Matsumura; Kentaroh Kitazawa; Seiya Terai; Takuya Kochi; Yutaka Ie; Masashi Nitani; Yoshio Aso; Fumitoshi Kakiuchi
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Publication Detail:
Type:  JOURNAL ARTICLE     Date:  2012-7-13
Journal Detail:
Title:  Organic letters     Volume:  -     ISSN:  1523-7052     ISO Abbreviation:  -     Publication Date:  2012 Jul 
Date Detail:
Created Date:  2012-7-16     Completed Date:  -     Revised Date:  -    
Medline Journal Info:
Nlm Unique ID:  100890393     Medline TA:  Org Lett     Country:  -    
Other Details:
Languages:  ENG     Pagination:  -     Citation Subset:  -    
Affiliation:
Department of Chemistry, Faculty of Science and Technology, Keio University , 3-14-1 Hiyoshi, Kohoku-ku, Yokohama, Kanagawa, 223-8522, Japan, and The Institute of Science and Industrial Research (ISIR), Osaka University , 8-1,7 Mihogaoka, Ibaraki, Osaka 567-0047, Japan.
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