Document Detail


Separation and recovery of nucleic acids with improved biological activity by acid-degradable polyacrylamide gel electrophoresis.
MedLine Citation:
PMID:  20419706     Owner:  NLM     Status:  MEDLINE    
Abstract/OtherAbstract:
One of the fundamental challenges in studying biomacromolecules (e.g. nucleic acids and proteins) and their complexes in a biological system is isolating them in their structurally and functionally intact forms. Electrophoresis offers convenient and efficient separation and analysis of biomacromolecules but recovery of separated biomacromolecules is a significant challenge. In this study, DNAs of various sizes were separated by electrophoresis in an acid-degradable polyacrylamide gel. Almost 100% of the nucleic acids were recovered after the identified gel bands were hydrolyzed under a mildly acidic condition and purified using anion exchange resin. Further concentration by centrifugal filtration and a second purification using ion exchange column chromatography yielded 44-84% of DNA. The second conventional (non-degradable) gel electrophoresis confirmed that the nucleic acids recovered from acid-degradable gel bands preserved their electrophoretic properties through acidic gel hydrolysis, purification, and concentration processes. The plasmid DNA recovered from acid-degradable gel transfected cells significantly more efficiently than the starting plasmid DNA (i.e. improved biological activity via acid-degradable PAGE). Separation of other types of nucleic acids such as small interfering RNA using this convenient and efficient technique was also demonstrated.
Authors:
Yoon Kyung Kim; Young Jik Kwon
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Publication Detail:
Type:  Journal Article    
Journal Detail:
Title:  Electrophoresis     Volume:  31     ISSN:  1522-2683     ISO Abbreviation:  Electrophoresis     Publication Date:  2010 May 
Date Detail:
Created Date:  2010-05-25     Completed Date:  2010-08-30     Revised Date:  -    
Medline Journal Info:
Nlm Unique ID:  8204476     Medline TA:  Electrophoresis     Country:  Germany    
Other Details:
Languages:  eng     Pagination:  1656-61     Citation Subset:  IM    
Affiliation:
Department of Biomedical Engineering, University of California, Irvine, CA, USA.
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MeSH Terms
Descriptor/Qualifier:
Animals
DNA / isolation & purification
Electrophoresis, Polyacrylamide Gel / methods*
Green Fluorescent Proteins
Hydrogen-Ion Concentration
Mice
Microscopy, Fluorescence
NIH 3T3 Cells
Nucleic Acids / isolation & purification*
Plasmids / isolation & purification
RNA, Small Interfering / isolation & purification
Transfection
Chemical
Reg. No./Substance:
0/Nucleic Acids; 0/RNA, Small Interfering; 147336-22-9/Green Fluorescent Proteins; 9007-49-2/DNA

From MEDLINE®/PubMed®, a database of the U.S. National Library of Medicine


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