| Rugged LC-MS/MS survey analysis for acrylamide in foods. | |
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MedLine Citation:
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PMID: 14664505 Owner: NLM Status: MEDLINE |
Abstract/OtherAbstract:
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The described liquid chromatography-tandem mass spectrometry (LC-MS/MS) method for the detection of acrylamide in food entails aqueous room temperature extraction, SPE cleanup, and analysis by LC-MS/MS. The method is applicable to a wide variety of foods. [(13)C(3)]acrylamide is the internal standard. The limit of quantitation is 10 ppb (microg/kg). Data were obtained in duplicate from >450 products representing >35 different food types. The variability in analyte levels in certain food types suggests that it may be possible to reduce acrylamide levels in those foods. |
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Authors:
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John A G Roach; Denis Andrzejewski; Martha L Gay; David Nortrup; Steven M Musser |
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Publication Detail:
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Type: Journal Article |
Journal Detail:
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Title: Journal of agricultural and food chemistry Volume: 51 ISSN: 0021-8561 ISO Abbreviation: J. Agric. Food Chem. Publication Date: 2003 Dec |
Date Detail:
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Created Date: 2003-12-10 Completed Date: 2004-01-21 Revised Date: 2007-11-15 |
Medline Journal Info:
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Nlm Unique ID: 0374755 Medline TA: J Agric Food Chem Country: United States |
Other Details:
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Languages: eng Pagination: 7547-54 Citation Subset: IM |
Affiliation:
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Center for Food Safety and Applied Nutrition, US Food and Drug Administration, 5100 Paint Branch Parkway, College Park, Maryland 20740, USA. jroach@cfsan.fda.gov |
Export Citation:
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APA/MLA Format Download EndNote Download BibTex |
| MeSH Terms | |
Descriptor/Qualifier:
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Acrylamide
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analysis* Bread / analysis Cereals / chemistry Chromatography, High Pressure Liquid / methods* Coffee / chemistry Food Analysis / methods* Food Contamination / analysis Mass Spectrometry / methods* Sensitivity and Specificity |
| Chemical | |
Reg. No./Substance:
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0/Coffee; 79-06-1/Acrylamide |
From MEDLINE®/PubMed®, a database of the U.S. National Library of Medicine
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