Document Detail

Routine use of natural abundance deuterium NMR in a polypeptidic chiral oriented solvent for the determination of the enantiomeric composition of chiral building blocks.
MedLine Citation:
PMID:  12000268     Owner:  NLM     Status:  MEDLINE    
[reaction: see text] Natural abundance deuterium 2D NMR spectroscopy in chiral liquid crystal was successfully used to efficiently analyze the enantiomeric composition of organic chiral building blocks involved in the syntheses of natural and synthetic bioactive products. The results reported here emphasize the high potential of this analytical strategy and prove its applicability for routinely determining enantiomeric excesses.
Arnaud Parenty; Jean-Marc Campagne; Christie Aroulanda; Philippe Lesot
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Publication Detail:
Type:  Journal Article    
Journal Detail:
Title:  Organic letters     Volume:  4     ISSN:  1523-7060     ISO Abbreviation:  Org. Lett.     Publication Date:  2002 May 
Date Detail:
Created Date:  2002-05-09     Completed Date:  2002-07-01     Revised Date:  -    
Medline Journal Info:
Nlm Unique ID:  100890393     Medline TA:  Org Lett     Country:  United States    
Other Details:
Languages:  eng     Pagination:  1663-6     Citation Subset:  IM    
ICSN-CNRS, Avenue de la Terrasse, 91198 Gif sur Yvette, France.
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MeSH Terms
Deuterium / chemistry
Indicators and Reagents
Magnetic Resonance Spectroscopy
Peptides / chemistry*
Reg. No./Substance:
0/Indicators and Reagents; 0/Peptides; 0/Solvents; 7782-39-0/Deuterium

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