Document Detail


Reagent for introducing pyrene residues in oligonucleotides.
MedLine Citation:
PMID:  1463786     Owner:  NLM     Status:  MEDLINE    
Abstract/OtherAbstract:
A novel pyrenyl-containing phosphoramidite reagent, N-[4-(1-pyrenyl)butyryl]-O1-(4,4'-dimethoxytrityl)-O2- [(diisopropylamino)(2-cyanoethoxy)phosphino]-3-amino-1 ,2-propanediol (5), has been synthesized from 4-(1-pyrenyl)butanoic acid in four steps with the 52% overall yield and used to incorporate pyrene residue(s) into oligonucleotides. Oligonucleotides 6 and 7, bearing one or two pyrenes at the 5'-terminus, have been prepared by means of that reagent, characterized with fluorescence spectra, and successfully used as primers in a polymerase chain reaction.
Authors:
V A Korshun; N B Pestov; K R Birikh; Y A Berlin
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Publication Detail:
Type:  Journal Article    
Journal Detail:
Title:  Bioconjugate chemistry     Volume:  3     ISSN:  1043-1802     ISO Abbreviation:  Bioconjug. Chem.     Publication Date:    1992 Nov-Dec
Date Detail:
Created Date:  1993-01-19     Completed Date:  1993-01-19     Revised Date:  2000-12-18    
Medline Journal Info:
Nlm Unique ID:  9010319     Medline TA:  Bioconjug Chem     Country:  UNITED STATES    
Other Details:
Languages:  eng     Pagination:  559-62     Citation Subset:  IM    
Affiliation:
M. M. Shemyakin Institute of Bioorganic Chemistry, Russian Academy of Sciences, Moscow.
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MeSH Terms
Descriptor/Qualifier:
Base Sequence
Electrophoresis, Polyacrylamide Gel
Indicators and Reagents*
Molecular Sequence Data
Oligonucleotides / chemistry*
Polymerase Chain Reaction
Pyrenes / chemistry*
Spectrometry, Fluorescence
Chemical
Reg. No./Substance:
0/Indicators and Reagents; 0/Oligonucleotides; 0/Pyrenes; 143039-35-4/N-(4-(1-pyrenyl)butyryl)-O(1)-(4,4'-dimethoxytrityl)-O(2)-((diisopropylamino)(2-cyanoethoxy)phosphino)-3-amino-1,2-propanediol

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