Document Detail


Reactions of sulfur and phosphorus substituted fluoroalkylating silicon reagents with imines and enamines under acidic conditions.
MedLine Citation:
PMID:  22283481     Owner:  NLM     Status:  Publisher    
Abstract/OtherAbstract:
Nucleophilic fluoroalkylation reactions of imines and enamines with alpha-phenylthio, alpha-phenylsulfonyl, and alpha-diethylphosphoryl substituted fluorinated silanes have been investigated. The reactions are promoted by hydrofluoric acid generated in situ from potassium hydrodifluoride and trifluoroacetic acid. Sulfur reagents worked well with both imines and enamines, while phosphorous reagent efficiently coupled only with enamines.
Authors:
Mikhail D Kosobokov; Alexander D Dilman; Marina I Struchkova; Pavel A Belyakov; Jinbo Hu
Publication Detail:
Type:  JOURNAL ARTICLE     Date:  2012-1-24
Journal Detail:
Title:  The Journal of organic chemistry     Volume:  -     ISSN:  1520-6904     ISO Abbreviation:  -     Publication Date:  2012 Jan 
Date Detail:
Created Date:  2012-1-30     Completed Date:  -     Revised Date:  -    
Medline Journal Info:
Nlm Unique ID:  2985193R     Medline TA:  J Org Chem     Country:  -    
Other Details:
Languages:  ENG     Pagination:  -     Citation Subset:  -    
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