Document Detail


Rapid reversed-phase liquid chromatographic determination of patulin in apple juice.
MedLine Citation:
PMID:  8680596     Owner:  NLM     Status:  MEDLINE    
Abstract/OtherAbstract:
A rapid, simple and economical method using a limited amount of organic solvent is described for the determination of patulin in apple juice. The sample was extracted with ethyl acetate and the extract was cleaned up by extraction with sodium carbonate solution. Patulin was then determined by reversed-phase liquid chromatography using a MicroPack C18 column and a variable-wavelength UV-Vis detector set at 276 nm. Patulin and 5-hydroxymethylfurfural were completely resolved by using water-acetonitrile (99:1, v/v) as the mobile phase at a flow-rate of 1.0 ml/min. The detection limit was < 5 micrograms/l and the recovery was 98%.
Authors:
V Gökmen; J Acar
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Publication Detail:
Type:  Journal Article    
Journal Detail:
Title:  Journal of chromatography. A     Volume:  730     ISSN:  0021-9673     ISO Abbreviation:  J Chromatogr A     Publication Date:  1996 Apr 
Date Detail:
Created Date:  1996-08-19     Completed Date:  1996-08-19     Revised Date:  2009-01-15    
Medline Journal Info:
Nlm Unique ID:  9318488     Medline TA:  J Chromatogr A     Country:  NETHERLANDS    
Other Details:
Languages:  eng     Pagination:  53-8     Citation Subset:  IM    
Affiliation:
Department of Food Engineering, Hacettepe University, Beytepe, Ankara, Turkey.
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MeSH Terms
Descriptor/Qualifier:
Beverages / analysis*
Chromatography, High Pressure Liquid / methods*,  statistics & numerical data
Food Contamination
Fruit*
Furaldehyde / analogs & derivatives,  analysis
Patulin / analysis*
Chemical
Reg. No./Substance:
149-29-1/Patulin; 67-47-0/5-hydroxymethylfurfural; 98-01-1/Furaldehyde

From MEDLINE®/PubMed®, a database of the U.S. National Library of Medicine


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