| Quasi in situ scanning force microscope with an automatic operated reaction chamber. | |
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MedLine Citation:
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PMID: 22128986 Owner: NLM Status: In-Data-Review |
Abstract/OtherAbstract:
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We describe the design and performance of a quasi in situ scanning force microscope with an automatic operated reaction chamber. The design provides a repetitive hermetically sealed sample environment for successive processing. The reaction chamber is based on a combination of a flexure-guided cover, a piezo-positioning system and a force applicator system. An axial force seals the cover against the reactor enabling flow-through applications at low pressure, ambient pressure, or elevated pressure. The position stability of the sample relative to the probe is characterized and a full automated operation of the instrument is explored by the alignment of an ABC terblock copolymer thin film undergoing solvent vapor annealing in the presence of a high electric field. Due to the high electric field strength and the sharp scanning force microscope tip it is impossible to perform in situ scanning in the presence of the electric field. |
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Authors:
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Markus Hund; Violetta Olszowka; Franz Fischer; Heinz Krejtschi |
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Publication Detail:
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Type: Journal Article |
Journal Detail:
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Title: The Review of scientific instruments Volume: 82 ISSN: 1089-7623 ISO Abbreviation: Rev Sci Instrum Publication Date: 2011 Nov |
Date Detail:
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Created Date: 2011-12-01 Completed Date: - Revised Date: - |
Medline Journal Info:
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Nlm Unique ID: 0405571 Medline TA: Rev Sci Instrum Country: United States |
Other Details:
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Languages: eng Pagination: 113709 Citation Subset: IM |
Affiliation:
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Lehrstuhl für Physikalische Chemie II, Universität Bayreuth, Bayreuth, GermanyLaboratory of Crystallography, University of Bayreuth, Bayreuth, GermanyZentrale Technik, Mechanik, Universität Bayreuth, Bayreuth, Germany. |
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From MEDLINE®/PubMed®, a database of the U.S. National Library of Medicine
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