Document Detail


Quasi in situ scanning force microscope with an automatic operated reaction chamber.
MedLine Citation:
PMID:  22128986     Owner:  NLM     Status:  In-Data-Review    
Abstract/OtherAbstract:
We describe the design and performance of a quasi in situ scanning force microscope with an automatic operated reaction chamber. The design provides a repetitive hermetically sealed sample environment for successive processing. The reaction chamber is based on a combination of a flexure-guided cover, a piezo-positioning system and a force applicator system. An axial force seals the cover against the reactor enabling flow-through applications at low pressure, ambient pressure, or elevated pressure. The position stability of the sample relative to the probe is characterized and a full automated operation of the instrument is explored by the alignment of an ABC terblock copolymer thin film undergoing solvent vapor annealing in the presence of a high electric field. Due to the high electric field strength and the sharp scanning force microscope tip it is impossible to perform in situ scanning in the presence of the electric field.
Authors:
Markus Hund; Violetta Olszowka; Franz Fischer; Heinz Krejtschi
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Publication Detail:
Type:  Journal Article    
Journal Detail:
Title:  The Review of scientific instruments     Volume:  82     ISSN:  1089-7623     ISO Abbreviation:  Rev Sci Instrum     Publication Date:  2011 Nov 
Date Detail:
Created Date:  2011-12-01     Completed Date:  -     Revised Date:  -    
Medline Journal Info:
Nlm Unique ID:  0405571     Medline TA:  Rev Sci Instrum     Country:  United States    
Other Details:
Languages:  eng     Pagination:  113709     Citation Subset:  IM    
Affiliation:
Lehrstuhl für Physikalische Chemie II, Universität Bayreuth, Bayreuth, GermanyLaboratory of Crystallography, University of Bayreuth, Bayreuth, GermanyZentrale Technik, Mechanik, Universität Bayreuth, Bayreuth, Germany.
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