Document Detail


Preparation and application of trimethylamine amination polychloromethyl styrene nanolatex coated capillary column for the determination of bromate by field-amplified sample stacking open-tubular capillary electrochromatography.
MedLine Citation:
PMID:  23456879     Owner:  NLM     Status:  MEDLINE    
Abstract/OtherAbstract:
A new trimethylamine amination polychloromethyl styrene nanolatex (TMAPL) and TMAPL coated capillary column (ccc-TMAPL) were successfully prepared. The TMAPL coating was characterized with reversed steady EOF values of ca. -16.8 × 10(-5) cm(2) V(-1) s(-1) . It was applied to establish open-tubular (OT) CEC and field-amplified sample stacking (FASS) OT-CEC methods for the determination of bromate in tap water. Compared to OT-CEC, the LOD with FASS-OT-CEC was improved from 80 to 8 ng/mL. The developed FASS-OT-CEC method was practically used for the analysis of bromate in tap water samples with recoveries ranging from 93.6 to 103.5%.
Authors:
Yaxiao Guo; Feifei Xu; Lei Meng; Wei Tang; Yan Xia; Yangjie Wu; Shusheng Zhang
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Publication Detail:
Type:  Evaluation Studies; Journal Article; Research Support, Non-U.S. Gov't     Date:  2013-04-14
Journal Detail:
Title:  Electrophoresis     Volume:  34     ISSN:  1522-2683     ISO Abbreviation:  Electrophoresis     Publication Date:  2013 May 
Date Detail:
Created Date:  2013-05-14     Completed Date:  2013-10-22     Revised Date:  2014-07-18    
Medline Journal Info:
Nlm Unique ID:  8204476     Medline TA:  Electrophoresis     Country:  Germany    
Other Details:
Languages:  eng     Pagination:  1312-8     Citation Subset:  IM    
Copyright Information:
© 2013 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.
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MeSH Terms
Descriptor/Qualifier:
Amination
Bromates / analysis*
Capillary Electrochromatography / instrumentation*
Drinking Water / analysis*
Halogenation
Methylamines / chemistry*
Nanostructures / chemistry
Reproducibility of Results
Sensitivity and Specificity
Styrene / chemistry*
Water Pollutants, Chemical / analysis*
Chemical
Reg. No./Substance:
0/Bromates; 0/Drinking Water; 0/Methylamines; 0/Water Pollutants, Chemical; 44LJ2U959V/Styrene; LHH7G8O305/trimethylamine
Comments/Corrections
Erratum In:
Electrophoresis. 2014 Feb;35(4):594

From MEDLINE®/PubMed®, a database of the U.S. National Library of Medicine


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