| Polyphosphoric Acid Promoted Synthesis of 10,11-Dihydrobenzo[j]fluoranthen-12-one. | |
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MedLine Citation:
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PMID: 22515182 Owner: NLM Status: Publisher |
Abstract/OtherAbstract:
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A straightforward synthesis of 3,8-dimethoxy-10,11-dihydrobenzo[j]fluoranthen-12-ones 1 is reported in a seven-step route from biphenyl-4,4'-diol 2 via the transformation of a double Claisen rearrangement, cross metathesis with ethyl acrylate, and polyphosphoric acid (PPA)-promoted Friedel-Crafts electrophilic benzannulation in good yields. |
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Authors:
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Meng-Yang Chang; Tein-Wei Lee; Ming-Hao Wu |
Publication Detail:
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Type: JOURNAL ARTICLE Date: 2012-4-19 |
Journal Detail:
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Title: Organic letters Volume: - ISSN: 1523-7052 ISO Abbreviation: - Publication Date: 2012 Apr |
Date Detail:
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Created Date: 2012-4-20 Completed Date: - Revised Date: - |
Medline Journal Info:
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Nlm Unique ID: 100890393 Medline TA: Org Lett Country: - |
Other Details:
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Languages: ENG Pagination: - Citation Subset: - |
Affiliation:
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Department of Medicinal and Applied Chemistry, Kaohsiung Medical University , Kaohsiung 807, Taiwan. |
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From MEDLINE®/PubMed®, a database of the U.S. National Library of Medicine
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