Document Detail


Polymorphism of natural fatty acid liquid crystalline phases.
MedLine Citation:
PMID:  22118375     Owner:  NLM     Status:  Publisher    
Abstract/OtherAbstract:
We study the phase behaviour in water of a mixture of natural long chain fatty acids (FAM) in association with ethylenediamine (EDA) and report a rich polymorphism depending on the composition. At a fixed EDA/FAM molar ratio, we observe upon dilution a succession of organized phases going from a lamellar phase to a hexagonal phase and finally, to cylindrical micelles. The phase structure is established using polarizing microscopy, SAXS and SANS. Interestingly, in the lamellar phase domain, we observe the presence of defects upon dilution, which SAXS shows to correspond to intra-bilayer correlations. NMR and FFTEM techniques suggest that these defects are related to an increase in the spontaneous curvature of the molecules monolayers in the lamellae. ATR-FTIR spectroscopy was also used to investigate the degree of ionization within these assemblies. The successive morphological transitions are discussed with regards to possible molecular mechanisms, in which the interaction between the acid surfactant and the amine counterion plays the leading role.
Authors:
Hélène Fay; Steven Meeker; Juliette Cayer-Barrioz; Denis Mazuyer; Isabelle Ly; Frédéric Nallet; Bernard Desbat; Jean-Paul Douliez; Virginie Ponsinet; Olivier Mondain-Monval
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Publication Detail:
Type:  JOURNAL ARTICLE     Date:  2011-11-28
Journal Detail:
Title:  Langmuir : the ACS journal of surfaces and colloids     Volume:  -     ISSN:  1520-5827     ISO Abbreviation:  -     Publication Date:  2011 Nov 
Date Detail:
Created Date:  2011-11-28     Completed Date:  -     Revised Date:  -    
Medline Journal Info:
Nlm Unique ID:  9882736     Medline TA:  Langmuir     Country:  -    
Other Details:
Languages:  ENG     Pagination:  -     Citation Subset:  -    
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