Document Detail


Polyketide origin of pheromones of Carpophilus davidsoni and C. mutilatus (Coleoptera: Nitidulidae).
MedLine Citation:
PMID:  8733623     Owner:  NLM     Status:  MEDLINE    
Abstract/OtherAbstract:
Biosynthesis of pheromones from Carpophilus davidsoni Dobson and C. mutilatus Erichson was investigated by feeding the beetles diets containing isotopically substituted (13C and deuterium) fatty acids and then analyzing the resulting labeled pheromone components. (2E,4E,6E,8E)-7-Ethyl-3,5-dimethyl-2,4,6,8-undecate traene, (2E,4E,6E,8E)-3,5,7-trimethyl-2,4,6,8-undecatetraen e and (2E,4E,6E)-5-ethyl-3-methyl-2,4,6-nonatriene from C. davidsoni and (3E,5E,7E)-5-ethyl-7-methyl-3,5,7-undecatriene from C. mutilatus were abundant enough to be analyzed by both NMR spectroscopy and MS. Eleven additional minor analogues were analyzed only by MS. Each hydrocarbon can be assembled from just three different acyl units: The initial unit can be acetate, propionate or butyrate. Propionate is the second unit in all of the analogues encountered so far, extending the chain by two carbons and producing a methyl branch. Subsequent chain-extending units can be either propionate or butyrate, leading to additional methyl or ethyl branches, respectively. The final acyl unit is either propionate or butyrate and it loses its carboxyl carbon during hydrocarbon biosynthesis. A hydrocarbon with four total units is a triene and one with five is a tetraene. Assembly is proposed to be as in usual fatty acid anabolism, except that other precursor units are used in addition to acetate and that the double-bond reduction step of each chain-elongation cycle does not occur, leaving the conjugated, unsaturated system. Seven of the analyzed hydrocarbons were not previously known to occur in C. davidsoni; two of these are novel: (2E,4E,6E,8E)-5,7-diethyl-3-methyl-2,4,6,8-undecate traene and (2E,4E,6E)-3,5-dimethyl-2,4,6-octatriene.
Authors:
R J Bartelt; D Weisleder
Related Documents :
383713 - Kinetics of the utilization of medium and long chain fatty acids by mutant of escherich...
20962873 - Microbial biodegradation of aromatic alkanoic naphthenic acids is affected by the degre...
22484833 - Use of quantitative microbiological analyses to trace origin of contamination of parent...
Publication Detail:
Type:  Journal Article    
Journal Detail:
Title:  Bioorganic & medicinal chemistry     Volume:  4     ISSN:  0968-0896     ISO Abbreviation:  Bioorg. Med. Chem.     Publication Date:  1996 Mar 
Date Detail:
Created Date:  1996-10-24     Completed Date:  1996-10-24     Revised Date:  2006-11-15    
Medline Journal Info:
Nlm Unique ID:  9413298     Medline TA:  Bioorg Med Chem     Country:  ENGLAND    
Other Details:
Languages:  eng     Pagination:  429-38     Citation Subset:  IM    
Affiliation:
Bioactive Constituents Unit, USDA Agricultural Research Service, National Center for Agricultural Utilization Research, Peoria, IL 61604, USA.
Export Citation:
APA/MLA Format     Download EndNote     Download BibTex
MeSH Terms
Descriptor/Qualifier:
Aldehydes / metabolism
Animals
Beetles / metabolism*
Female
Magnetic Resonance Spectroscopy
Male
Mass Spectrometry
Propionates
Sex Attractants / biosynthesis*
Chemical
Reg. No./Substance:
0/Aldehydes; 0/Propionates; 0/Sex Attractants; 124-25-4/tetradecanal

From MEDLINE®/PubMed®, a database of the U.S. National Library of Medicine


Previous Document:  Asymmetric aldol condensation as a route to polypropionate derived pheromones.
Next Document:  Synthesis of [14,14,14-2H3] 12-hydroxytetradecanoic acid and [13,14-2H2] 11-hydroxytetradecanoic aci...