Document Detail


One- and two-dimensional 1H magic-angle spinning experiments on hydrous silicate glasses.
MedLine Citation:
PMID:  8748647     Owner:  NLM     Status:  MEDLINE    
Abstract/OtherAbstract:
Applications of various one- and two-dimensional 1H magic-angle spinning nuclear magnetic resonance (MAS NMR) techniques for the elucidation of structural properties of hydrous silicate glasses are described. Advantages and limitations of one-dimensional experiments [MAS and combined rotation and multiple-puls spectroscopy (CRAMPS)] and of two-dimensional approaches (spin-exchange experiments, "MAS-CRAMPS" correlation plus extended versions) are discussed. The various 1H MAS NMR techniques are illustrated by practical examples of spectra obtained from a hydrous silicate glass of Na2O.4SiO2.0.7H2O composition.
Authors:
T Schaller; A Sebald
Related Documents :
15649747 - Separated quadrupolar field experiment.
1623127 - A general approach for determining scalar coupling constants in polypeptides and proteins.
9053117 - 31p-19f rotational-echo, double-resonance nuclear magnetic resonance experiment on fluo...
7240647 - A 13c-nmr study of non-planar distortions in amides.
21894947 - Screw dislocation-driven growth of 2d nanoplates.
23136957 - Luminescent properties of metal-organic framework mof-5: relativistic time-dependent de...
Publication Detail:
Type:  Journal Article; Research Support, Non-U.S. Gov't    
Journal Detail:
Title:  Solid state nuclear magnetic resonance     Volume:  5     ISSN:  0926-2040     ISO Abbreviation:  Solid State Nucl Magn Reson     Publication Date:  1995 Oct 
Date Detail:
Created Date:  1996-10-23     Completed Date:  1996-10-23     Revised Date:  2006-11-15    
Medline Journal Info:
Nlm Unique ID:  9306181     Medline TA:  Solid State Nucl Magn Reson     Country:  NETHERLANDS    
Other Details:
Languages:  eng     Pagination:  89-102     Citation Subset:  IM    
Affiliation:
Bayerisches Geoinstitut, Universität Bayreuth, Germany.
Export Citation:
APA/MLA Format     Download EndNote     Download BibTex
MeSH Terms
Descriptor/Qualifier:
Glass / chemistry*
Magnetic Resonance Spectroscopy / methods*
Protons
Silicates / chemistry*
Water / chemistry
Chemical
Reg. No./Substance:
0/Protons; 0/Silicates; 7732-18-5/Water

From MEDLINE®/PubMed®, a database of the U.S. National Library of Medicine


Previous Document:  27Al magic-angle spinning nuclear magnetic resonance satellite transition spectroscopy of glasses in...
Next Document:  6Li nuclear magnetic resonance chemical shifts, coordination number and relaxation in crystalline an...