Document Detail

One-dimensional double-quantum magic-angle-spinning NMR of deuterated solids.
MedLine Citation:
PMID:  7827966     Owner:  NLM     Status:  MEDLINE    
An approach to double-quantum magic-angle spinning (2Q-MAS) of spin I = 1 with a time-share irradiation, resulting in a one-dimensional (1D) MQ spectrum, is demonstrated in this paper. The experiment was carried out with perdeuterated dimethoxybenzene and showed that the 2Q transitions were insensitive to the spinning axis deviation from the magic angle. The 1D-2Q-MAS scheme may also be applied to nitrogen-containing solids.
D Yang; C Ye
Related Documents :
16471486 - Cross-correlated relaxation between h1' chemical shift anisotropy and h1'-h2' dipolar r...
22344326 - New magnetic phase diagram of (sr,ca)(2)ruo(4).
15638536 - Structural aspects in semicrystalline samples of the mannan ii family.
9340006 - Eseem study of the phyllosemiquinone radical a1.- in 14n- and 15n-labeled photosystem i.
24059686 - Growth of crystalline hydroxyapatite thin films at room temperature by tuning the energ...
18315176 - Study on an azimuthal line cusp ion source for the kstar neutral beam injector.
Publication Detail:
Type:  Journal Article; Research Support, Non-U.S. Gov't    
Journal Detail:
Title:  Solid state nuclear magnetic resonance     Volume:  2     ISSN:  0926-2040     ISO Abbreviation:  Solid State Nucl Magn Reson     Publication Date:  1993 Sep 
Date Detail:
Created Date:  1995-02-22     Completed Date:  1995-02-22     Revised Date:  2006-11-15    
Medline Journal Info:
Nlm Unique ID:  9306181     Medline TA:  Solid State Nucl Magn Reson     Country:  NETHERLANDS    
Other Details:
Languages:  eng     Pagination:  147-50     Citation Subset:  IM    
Laboratory of Magnetic Resonance and Atomic and Molecular Physics, Wuhan Institute of Physics, Chinese Academy of Sciences, China.
Export Citation:
APA/MLA Format     Download EndNote     Download BibTex
MeSH Terms
Anisoles / chemistry
Magnetic Resonance Spectroscopy / methods*
Reg. No./Substance:
0/Anisoles; 7782-39-0/Deuterium

From MEDLINE®/PubMed®, a database of the U.S. National Library of Medicine

Previous Document:  Adhesion molecule deficiencies and their clinical significance.
Next Document:  High-resolution 1H NMR in solids with frequency-switched multiple-pulse sequences.