| One-dimensional double-quantum magic-angle-spinning NMR of deuterated solids. | |
| | |
MedLine Citation:
|
PMID: 7827966 Owner: NLM Status: MEDLINE |
Abstract/OtherAbstract:
|
An approach to double-quantum magic-angle spinning (2Q-MAS) of spin I = 1 with a time-share irradiation, resulting in a one-dimensional (1D) MQ spectrum, is demonstrated in this paper. The experiment was carried out with perdeuterated dimethoxybenzene and showed that the 2Q transitions were insensitive to the spinning axis deviation from the magic angle. The 1D-2Q-MAS scheme may also be applied to nitrogen-containing solids. |
| | |
Authors:
|
D Yang; C Ye |
Related Documents
:
|
16471486 - Cross-correlated relaxation between h1' chemical shift anisotropy and h1'-h2' dipolar r... 22344326 - New magnetic phase diagram of (sr,ca)(2)ruo(4). 15638536 - Structural aspects in semicrystalline samples of the mannan ii family. 9340006 - Eseem study of the phyllosemiquinone radical a1.- in 14n- and 15n-labeled photosystem i. 18315176 - Study on an azimuthal line cusp ion source for the kstar neutral beam injector. 16683586 - Changes in uranium speciation through a depth sequence of contaminated hanford sediments. |
Publication Detail:
|
Type: Journal Article; Research Support, Non-U.S. Gov't |
Journal Detail:
|
Title: Solid state nuclear magnetic resonance Volume: 2 ISSN: 0926-2040 ISO Abbreviation: Solid State Nucl Magn Reson Publication Date: 1993 Sep |
Date Detail:
|
Created Date: 1995-02-22 Completed Date: 1995-02-22 Revised Date: 2006-11-15 |
Medline Journal Info:
|
Nlm Unique ID: 9306181 Medline TA: Solid State Nucl Magn Reson Country: NETHERLANDS |
Other Details:
|
Languages: eng Pagination: 147-50 Citation Subset: IM |
Affiliation:
|
Laboratory of Magnetic Resonance and Atomic and Molecular Physics, Wuhan Institute of Physics, Chinese Academy of Sciences, China. |
Export Citation:
|
APA/MLA Format Download EndNote Download BibTex |
| MeSH Terms | |
Descriptor/Qualifier:
|
Anisoles
/
chemistry Deuterium Magnetic Resonance Spectroscopy / methods* |
| Chemical | |
Reg. No./Substance:
|
0/Anisoles; 7782-39-0/Deuterium |
From MEDLINE®/PubMed®, a database of the U.S. National Library of Medicine
Previous Document: Adhesion molecule deficiencies and their clinical significance.
Next Document: High-resolution 1H NMR in solids with frequency-switched multiple-pulse sequences.