Document Detail


One-dimensional double-quantum magic-angle-spinning NMR of deuterated solids.
MedLine Citation:
PMID:  7827966     Owner:  NLM     Status:  MEDLINE    
Abstract/OtherAbstract:
An approach to double-quantum magic-angle spinning (2Q-MAS) of spin I = 1 with a time-share irradiation, resulting in a one-dimensional (1D) MQ spectrum, is demonstrated in this paper. The experiment was carried out with perdeuterated dimethoxybenzene and showed that the 2Q transitions were insensitive to the spinning axis deviation from the magic angle. The 1D-2Q-MAS scheme may also be applied to nitrogen-containing solids.
Authors:
D Yang; C Ye
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Publication Detail:
Type:  Journal Article; Research Support, Non-U.S. Gov't    
Journal Detail:
Title:  Solid state nuclear magnetic resonance     Volume:  2     ISSN:  0926-2040     ISO Abbreviation:  Solid State Nucl Magn Reson     Publication Date:  1993 Sep 
Date Detail:
Created Date:  1995-02-22     Completed Date:  1995-02-22     Revised Date:  2006-11-15    
Medline Journal Info:
Nlm Unique ID:  9306181     Medline TA:  Solid State Nucl Magn Reson     Country:  NETHERLANDS    
Other Details:
Languages:  eng     Pagination:  147-50     Citation Subset:  IM    
Affiliation:
Laboratory of Magnetic Resonance and Atomic and Molecular Physics, Wuhan Institute of Physics, Chinese Academy of Sciences, China.
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MeSH Terms
Descriptor/Qualifier:
Anisoles / chemistry
Deuterium
Magnetic Resonance Spectroscopy / methods*
Chemical
Reg. No./Substance:
0/Anisoles; 7782-39-0/Deuterium

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