Document Detail

Note: Application of a pixel-array area detector to simultaneous single crystal x-ray diffraction and x-ray absorption spectroscopy measurements.
MedLine Citation:
PMID:  24784687     Owner:  NLM     Status:  Publisher    
X-ray diffraction (XRD) and X-ray absorption spectroscopy (XAS) are two main x-ray techniques in synchrotron radiation facilities. In this Note, we present an experimental setup capable of performing simultaneous XRD and XAS measurements by the application of a pixel-array area detector. For XRD, the momentum transfer in specular diffraction was measured by scanning the X-ray energy with fixed incoming and outgoing x-ray angles. By selecting a small fixed region of the detector to collect the XRD signal, the rest of the area was available for collecting the x-ray fluorescence for XAS measurements. The simultaneous measurement of XRD and X-ray absorption near edge structure for Pr0.67Sr0.33MnO3 film was demonstrated as a proof of principle for future time-resolved pump-probe measurements. A static sample makes it easy to maintain an accurate overlap of the X-ray spot and laser pump beam.
Cheng-Jun Sun; Bangmin Zhang; Dale L Brewe; Jing-Sheng Chen; G M Chow; T Venkatesan; Steve M Heald
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Publication Detail:
Journal Detail:
Title:  The Review of scientific instruments     Volume:  85     ISSN:  1089-7623     ISO Abbreviation:  Rev Sci Instrum     Publication Date:  2014 Apr 
Date Detail:
Created Date:  2014-5-2     Completed Date:  -     Revised Date:  -    
Medline Journal Info:
Nlm Unique ID:  0405571     Medline TA:  Rev Sci Instrum     Country:  -    
Other Details:
Languages:  ENG     Pagination:  046109     Citation Subset:  -    
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