| A New Class of Heterocycles: 1,4,3,5-Oxathiadiazepane 4,4-dioxides. | |
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MedLine Citation:
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PMID: 22334067 Owner: NLM Status: In-Data-Review |
Abstract/OtherAbstract:
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This work reports the synthesis of novel 1,4,3,5-oxathiadiazepanes 4,4-dioxides from the reaction of N'-benzyl-N-(2-hydroxyethyl)-sarcosine or proline sulfamide with aromatic aldehydes under acid catalysis. To prepare the starting materials N-Boc-sulfamide derivatives of sarcosine or proline were alkylated with benzyl alcohol under Mitsunobu reaction conditions, the Boc group was removed chemoselectively by acidolysis, and the resulting product reduced to the corresponding alcohol in good yields. |
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Authors:
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Amel Bendjeddou; Tahar Abbaz; Zine Regainia; Nour-Eddine Aouf |
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Publication Detail:
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Type: Journal Article Date: 2012-02-14 |
Journal Detail:
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Title: Molecules (Basel, Switzerland) Volume: 17 ISSN: 1420-3049 ISO Abbreviation: Molecules Publication Date: 2012 |
Date Detail:
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Created Date: 2012-02-15 Completed Date: - Revised Date: - |
Medline Journal Info:
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Nlm Unique ID: 100964009 Medline TA: Molecules Country: Switzerland |
Other Details:
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Languages: eng Pagination: 1890-9 Citation Subset: IM |
Affiliation:
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Laboratoire de Chimie Organique Appliquée, Groupe de chimie Hétérocyclique, Département de Chimie, Faculté des Sciences, Université d'Annaba, BP 12, 23000, Algérie. bendjeddouamel@gmail.com. |
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From MEDLINE®/PubMed®, a database of the U.S. National Library of Medicine
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