Document Detail


Microwave synthesis of poly(L-lactic acid).
MedLine Citation:
PMID:  19105899     Owner:  NLM     Status:  MEDLINE    
Abstract/OtherAbstract:
Synthesis of poly(L-lactic acid) typically requires a long process time with the use of tin octoate as a catalyst. In this study microwave-assisted polymerization of lactic acid has been studied both with the aid and without the aid of tin octoate catalyst. While the presence of tin octoate assists in the polymerization process, it is not a pre-requisite to polymerization with microwaves. Molecular masses in excess of 25 kDa were possible over process times as little as 2.5 h without the need for a controlled environment. Fourier-transform infrared spectroscopy, proton nuclear magnetic resonance spectroscopy and gel-permeation chromatography were used to follow the polymerization process. Microwave-assisted polymerization of lactic acid to yield poly(L-lactic acid) has been shown to be a viable and quicker alternative to tradition approaches to the synthesis of poly(L-lactic acid).
Authors:
Anurag Pandey; Pranesh B Aswath
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Publication Detail:
Type:  Journal Article; Research Support, Non-U.S. Gov't    
Journal Detail:
Title:  Journal of biomaterials science. Polymer edition     Volume:  20     ISSN:  0920-5063     ISO Abbreviation:  J Biomater Sci Polym Ed     Publication Date:  2009  
Date Detail:
Created Date:  2008-12-24     Completed Date:  2009-02-24     Revised Date:  -    
Medline Journal Info:
Nlm Unique ID:  9007393     Medline TA:  J Biomater Sci Polym Ed     Country:  Netherlands    
Other Details:
Languages:  eng     Pagination:  33-48     Citation Subset:  IM    
Affiliation:
Materials Science and Engineering Department, 500 West First Street, Room 325, University of Texas at Arlington, Arlington, TX 76019, USA.
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MeSH Terms
Descriptor/Qualifier:
Lactic Acid / chemical synthesis*,  chemistry
Microwaves*
Polymers / chemical synthesis*,  chemistry
Spectroscopy, Fourier Transform Infrared
Tin Compounds / chemistry
Chemical
Reg. No./Substance:
0/Polymers; 0/Tin Compounds; 26100-51-6/poly(lactic acid); 50-21-5/Lactic Acid

From MEDLINE®/PubMed®, a database of the U.S. National Library of Medicine


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