Document Detail


Micro-raman assessment of the ratio of carbon-carbon double bonds of two adhesive systems cured with LED or halogen light-curing units.
MedLine Citation:
PMID:  20157649     Owner:  NLM     Status:  In-Process    
Abstract/OtherAbstract:
PURPOSE: the purpose of the study was to compare the ratio of carbon-carbon double bonds (RDB) of two adhesive systems cured by five different light-curing units (LCUs) using micro-Raman spectroscopy. materials and methods: ten samples of an etch-and-rinse (Excite), a two-step self-etching adhesive system (AdheSE) - ie, primer and bond mixed - and AdheSE Bond only were prepared and cured with one of the following LEDs: Elipar Freelight2; Bluephase; SmartLite; Coltolux, each for 10 s; or a conventional halogen Prismetics Lite for 10 s or 20 s. Micro-Raman spectra were obtained from uncured and cured samples of all three groups to calculate the RDB. Data were statistically analyzed using ANOVA.
RESULTS: the mean RDB values were 62% to 76% (Excite), 36% to 50% (AdheSE Primer+Bond) and 58% to 63% (AdheSE Bond). At 20 s, Prismetics Lite produced significantly higher RDB in Excite than the other LCUs and Prismetics Lite at 10 s (p < 0.05). Prismetics Lite at 20 s and Elipar produced comparable RDB values of AdheSE Bond and AdheSE Primer+Bond (p > 0.05). Excite showed significantly higher RDB values than AdheSE (p < 0.05) whilst AdheSE Bond showed significantly higher RDB than AdheSE Primer+Bond (p < 0.05).
CONCLUSION: the etch-and-rinse adhesive cured with the halogen LCU for 20 s gave higher conversion than LED LCUs or halogen for 10 s curing time. The highest intensity LED [Elipar] produced higher or comparable conversion compared to the lower intensity LED LCUs for the same curing time. The etch-and-rinse adhesive showed higher RDB than the self-etching adhesive system. The presence of the primer in the self-etching adhesive compromised polymerisation.
Authors:
Vesna Miletic; Ario Santini
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Publication Detail:
Type:  Journal Article    
Journal Detail:
Title:  The journal of adhesive dentistry     Volume:  12     ISSN:  1461-5185     ISO Abbreviation:  J Adhes Dent     Publication Date:  2010 Dec 
Date Detail:
Created Date:  2011-01-19     Completed Date:  -     Revised Date:  -    
Medline Journal Info:
Nlm Unique ID:  100888552     Medline TA:  J Adhes Dent     Country:  England    
Other Details:
Languages:  eng     Pagination:  461-7     Citation Subset:  D    
Affiliation:
Edinburgh Postgraduate Dental Institute, The University of Edinburgh, UK. vesna.miletic@gmail.com
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