Document Detail


Luminescent molecular Ag-S nanocluster [Ag(62)S(13)(SBu(t))(32)](BF(4))(4).
MedLine Citation:
PMID:  21114326     Owner:  NLM     Status:  In-Process    
Abstract/OtherAbstract:
The first observation of luminescence from a structurally well-defined Ag(2)S molecular nanocluster is reported. Reaction of AgSBu(t)/AgBF(4) with N(2)H(4) in methanol affords the tetracationic cluster [Ag(62)S(13)(SBu(t))(32)](BF(4))(4), which has a core-shell configuration. The 14 silver(I) centers of the [Ag(14)S(13)] core are in a face-centered cubic arrangement with each edge bridged by a S(2-) ligand; the core is further connected to the [Ag(48)(SBu(t))(32)] shell via both Ag-S bonds and Ag···Ag interactions. This novel cluster displays intense red emission in both the solid state and solution at room temperature.
Authors:
Gen Li; Zhen Lei; Quan-Ming Wang
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Publication Detail:
Type:  Journal Article     Date:  2010-11-29
Journal Detail:
Title:  Journal of the American Chemical Society     Volume:  132     ISSN:  1520-5126     ISO Abbreviation:  J. Am. Chem. Soc.     Publication Date:  2010 Dec 
Date Detail:
Created Date:  2010-12-15     Completed Date:  -     Revised Date:  -    
Medline Journal Info:
Nlm Unique ID:  7503056     Medline TA:  J Am Chem Soc     Country:  United States    
Other Details:
Languages:  eng     Pagination:  17678-9     Citation Subset:  -    
Affiliation:
State Key Laboratory of Physical Chemistry of Solid Surfaces, Department of Chemistry, College of Chemistry and Chemical Engineering, Xiamen University, Xiamen, Fujian 361005, PR China.
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