Document Detail


Increased ELISA sensitivity using a modified extraction buffer for detection of Xanthomonas campestris pv. vesicatoria in leaf tissue.
MedLine Citation:
PMID:  9351221     Owner:  NLM     Status:  MEDLINE    
Abstract/OtherAbstract:
In vitro and in planta sensitivity of an indirect enzyme-linked immunoassay technique, using a monoclonal antibody specific for the lipopolysaccharide (LPS) of Xanthomonas campestris pv. vesicatoria, was increased 10-fold by using a new extraction buffer (gl of: KH2PO4, 2; NaHPO4, 11.5; EDTA disodium, 0.14; thimerosal, 0.02; and lysozyme, 0.2). The procedure improved sensitivity without increasing background levels. In vitro, the limit of detection was between 1 x 10(7) and 1 x 10(8) cells ml-1 with the conventional extraction buffer phosphate-buffered saline (PBS) and less than 1 x 10(6) cells ml-1 when lysozyme extraction buffer was substituted for PBS. In comparing 22 X. c. vesicatoria strains, absorbance readings were increased close to three-fold with the lysozyme extraction buffer as opposed to PBS. When leaf tissue extract was spiked with the bacterium, the limit of detection was 1 x 10(7) cfu ml-1 and 1 x 10(8) cfu ml-1 with the lysozyme solution and PBS, respectively, as the extraction buffers. When using the lysozyme extraction buffer in combination with a commercial amplification system, the limit of detection was decreased to less than 1 x 10(5) cfu ml-1 in leaf tissue. The addition of the lysozyme and EDTA to the phosphate buffer resulted in release of a significant quantity of LPS and concomitant dramatic increase in sensitivity. The new procedure, termed lysozyme ELISA (L-ELISA), should increase sensitivity of ELISA reactions where LPS is the reacting epitope.
Authors:
J B Jones; G C Somodi; J W Scott
Publication Detail:
Type:  Journal Article; Research Support, U.S. Gov't, Non-P.H.S.    
Journal Detail:
Title:  Journal of applied microbiology     Volume:  83     ISSN:  1364-5072     ISO Abbreviation:  J. Appl. Microbiol.     Publication Date:  1997 Oct 
Date Detail:
Created Date:  1998-02-10     Completed Date:  1998-02-10     Revised Date:  2006-11-15    
Medline Journal Info:
Nlm Unique ID:  9706280     Medline TA:  J Appl Microbiol     Country:  ENGLAND    
Other Details:
Languages:  eng     Pagination:  397-401     Citation Subset:  IM    
Affiliation:
University of Florida, Gulf Coast Research and Education Center, Bradenton 34203, USA.
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MeSH Terms
Descriptor/Qualifier:
Antigens, Bacterial / immunology
Buffers
Edetic Acid / chemistry
Enzyme-Linked Immunosorbent Assay / methods*
Lipopolysaccharides / immunology
Muramidase / chemistry
Plant Leaves / microbiology
Sensitivity and Specificity
Xanthomonas campestris / immunology,  isolation & purification*
Chemical
Reg. No./Substance:
0/Antigens, Bacterial; 0/Buffers; 0/Lipopolysaccharides; 60-00-4/Edetic Acid; EC 3.2.1.17/Muramidase

From MEDLINE®/PubMed®, a database of the U.S. National Library of Medicine


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