Document Detail


Gas-liquid chromatographic determination of nikethamide in injectable preparations.
MedLine Citation:
PMID:  1249047     Owner:  NLM     Status:  MEDLINE    
Abstract/OtherAbstract:
A gas-liquid chromatographic (GLC) method, using a 4% XE-60 on 80-100 mesh Gas-Chrom Q column, a flame ionization detector, and anthracene as the internal standard, has been developed for the direct determination of nikethamide. Eight collaborators analyzed 4 samples, using methanol as the solvent; the coefficients of variation obtained ranged from 1.19 to 3.20%. In a limited study with acetone as the solvent, the coefficients of variation ranged from 0.59 to 1.96%. The GLC method with acetone as a solvent has been adopted as official first action.
Authors:
J M Newton
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Publication Detail:
Type:  Journal Article    
Journal Detail:
Title:  Journal - Association of Official Analytical Chemists     Volume:  59     ISSN:  0004-5756     ISO Abbreviation:  J Assoc Off Anal Chem     Publication Date:  1976 Jan 
Date Detail:
Created Date:  1976-04-10     Completed Date:  1976-04-10     Revised Date:  2009-10-27    
Medline Journal Info:
Nlm Unique ID:  7505559     Medline TA:  J Assoc Off Anal Chem     Country:  UNITED STATES    
Other Details:
Languages:  eng     Pagination:  93-7     Citation Subset:  IM    
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MeSH Terms
Descriptor/Qualifier:
Chromatography, Gas / methods*
Microchemistry
Nikethamide / analysis*
Solutions / analysis
Solvents
Chemical
Reg. No./Substance:
0/Solutions; 0/Solvents; 59-26-7/Nikethamide

From MEDLINE®/PubMed®, a database of the U.S. National Library of Medicine


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