| Gas-liquid chromatographic determination of nikethamide in injectable preparations. | |
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MedLine Citation:
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PMID: 1249047 Owner: NLM Status: MEDLINE |
Abstract/OtherAbstract:
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A gas-liquid chromatographic (GLC) method, using a 4% XE-60 on 80-100 mesh Gas-Chrom Q column, a flame ionization detector, and anthracene as the internal standard, has been developed for the direct determination of nikethamide. Eight collaborators analyzed 4 samples, using methanol as the solvent; the coefficients of variation obtained ranged from 1.19 to 3.20%. In a limited study with acetone as the solvent, the coefficients of variation ranged from 0.59 to 1.96%. The GLC method with acetone as a solvent has been adopted as official first action. |
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Authors:
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J M Newton |
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Publication Detail:
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Type: Journal Article |
Journal Detail:
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Title: Journal - Association of Official Analytical Chemists Volume: 59 ISSN: 0004-5756 ISO Abbreviation: J Assoc Off Anal Chem Publication Date: 1976 Jan |
Date Detail:
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Created Date: 1976-04-10 Completed Date: 1976-04-10 Revised Date: 2009-10-27 |
Medline Journal Info:
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Nlm Unique ID: 7505559 Medline TA: J Assoc Off Anal Chem Country: UNITED STATES |
Other Details:
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Languages: eng Pagination: 93-7 Citation Subset: IM |
Export Citation:
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APA/MLA Format Download EndNote Download BibTex |
| MeSH Terms | |
Descriptor/Qualifier:
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Chromatography, Gas
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methods* Microchemistry Nikethamide / analysis* Solutions / analysis Solvents |
| Chemical | |
Reg. No./Substance:
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0/Solutions; 0/Solvents; 59-26-7/Nikethamide |
From MEDLINE®/PubMed®, a database of the U.S. National Library of Medicine
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