Document Detail


From polymer to size-defined oligomers: a step economy process for the efficient and stereocontrolled construction of chondroitin oligosaccharides and biotinylated conjugates thereof: part 1.
MedLine Citation:
PMID:  19575349     Owner:  NLM     Status:  MEDLINE    
Abstract/OtherAbstract:
Controlled acid hydrolysis of polymeric chondroitin sulfate of bovine origin afforded in good yield a basic disaccharide fragment that was used for the first time as a starting material for the expeditious preparation of a set of building blocks that in turn act as versatile synthons for the efficient and stereocontrolled construction of a collection of size-defined chondroitin oligomers (from di- to octasaccharides). This step economy process allows their preparation as reducing species, fitted with a fluorophore, or as biotinylated conjugates; all useful tools for the preparation of microarrays, or as probes for the study of the biosynthesis of chondroitin sulfate.
Authors:
Aude Vibert; Chrystel Lopin-Bon; Jean-Claude Jacquinet
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Publication Detail:
Type:  Journal Article; Research Support, Non-U.S. Gov't    
Journal Detail:
Title:  Chemistry (Weinheim an der Bergstrasse, Germany)     Volume:  15     ISSN:  1521-3765     ISO Abbreviation:  Chemistry     Publication Date:  2009 Sep 
Date Detail:
Created Date:  2009-09-21     Completed Date:  2010-01-04     Revised Date:  -    
Medline Journal Info:
Nlm Unique ID:  9513783     Medline TA:  Chemistry     Country:  Germany    
Other Details:
Languages:  eng     Pagination:  9561-78     Citation Subset:  IM    
Affiliation:
Institut de Chimie Organique et Analytique, UMR 6005 Universit?? d'Orl??ans et CNRS, Universit?? d'Orl??ans, BP 6759, 45067 Orl??ans Cedex, France.
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MeSH Terms
Descriptor/Qualifier:
Animals
Biotinylation
Cattle
Chondroitin Sulfates / chemistry*
Glycosylation
Oligosaccharides / chemical synthesis,  chemistry*
Polymers / chemical synthesis*,  chemistry
Stereoisomerism
Chemical
Reg. No./Substance:
0/Oligosaccharides; 0/Polymers; 9007-28-7/Chondroitin Sulfates

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