Document Detail

Formation of self-assembled organosilicon-functionalized quinquethiophene monolayers by fast processing techniques.
MedLine Citation:
PMID:  23036156     Owner:  NLM     Status:  Publisher    
Different techniques for a relatively fast self-assembled monolayer film formation such as Langmuir-Blodgett (LB), spin-coating and dip-coating methods have been compared using chloro[11-(5''''-ethyl-2,2':5',2'':5'',2''':5''',2''''-quinquethiophene-5-yl)undecyl]dimethylsilane as a reactive precursor. It was shown that both spin-coating and LB techniques are very promising methods for preparation of highly ordered monolayer films of organosilicon-functionalized quinquethiophene with vertical orientation of oligothiophene fragments, while dip-coating gives only partial coverage. Optimal conditions for complete filling out the substrate surface by the quinquethiophene-containing monolayer by spin-coating and LB methods have been found. Grazing incidence X-ray diffraction measurements confirmed formation of in-plane crystalline order within the monolayer film. Changes in the layer structure were established by X-Ray reflectivity and Grazing Incidence X-Ray Diffraction methods.
Elena V Agina; Ivan Usov; Oleg V Borshchev; Jingbo Wang; Ahmed Mourran; Maxim A Shcherbina; Artem V Bakirov; Souren Grigorian; Martin Möller; Sergei N Chvalun; Sergei A Ponomarenko
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Publication Detail:
Type:  JOURNAL ARTICLE     Date:  2012-10-4
Journal Detail:
Title:  Langmuir : the ACS journal of surfaces and colloids     Volume:  -     ISSN:  1520-5827     ISO Abbreviation:  Langmuir     Publication Date:  2012 Oct 
Date Detail:
Created Date:  2012-10-5     Completed Date:  -     Revised Date:  -    
Medline Journal Info:
Nlm Unique ID:  9882736     Medline TA:  Langmuir     Country:  -    
Other Details:
Languages:  ENG     Pagination:  -     Citation Subset:  -    
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