Document Detail

Fluorous Mixture Synthesis of Four Stereoisomers of the C21-C40 Fragment of Tetrafibricin.
MedLine Citation:
PMID:  20686632     Owner:  NLM     Status:  Publisher    
Four stereoisomers of the C21-C40 fragment are synthesized in a single exercise with the aid of fluorous tagging to encode configurations at C37 and C33. After demixing and detagging, the isomers were found to have substantially identical (1)H NMR spectra. However, there were some small but reliable differences in their (13)C NMR spectra.
Kai Zhang; Dennis P Curran
Publication Detail:
Journal Detail:
Title:  Synlett : accounts and rapid communications in synthetic organic chemistry     Volume:  2010     ISSN:  0936-5214     ISO Abbreviation:  -     Publication Date:  2010 Mar 
Date Detail:
Created Date:  2010-8-5     Completed Date:  -     Revised Date:  -    
Medline Journal Info:
Nlm Unique ID:  9203577     Medline TA:  Synlett     Country:  -    
Other Details:
Languages:  ENG     Pagination:  667-674     Citation Subset:  -    
Department of Chemistry, University of Pittsburgh, Pittsburgh, PA 15260, USA Fax +1(412)6249861.
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Grant Support
R37 GM033372-26//NIGMS NIH HHS

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