| Fluorous Mixture Synthesis of Four Stereoisomers of the C21-C40 Fragment of Tetrafibricin. | |
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MedLine Citation:
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PMID: 20686632 Owner: NLM Status: Publisher |
Abstract/OtherAbstract:
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Four stereoisomers of the C21-C40 fragment are synthesized in a single exercise with the aid of fluorous tagging to encode configurations at C37 and C33. After demixing and detagging, the isomers were found to have substantially identical (1)H NMR spectra. However, there were some small but reliable differences in their (13)C NMR spectra. |
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Authors:
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Kai Zhang; Dennis P Curran |
Publication Detail:
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Type: JOURNAL ARTICLE |
Journal Detail:
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Title: Synlett : accounts and rapid communications in synthetic organic chemistry Volume: 2010 ISSN: 0936-5214 ISO Abbreviation: - Publication Date: 2010 Mar |
Date Detail:
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Created Date: 2010-8-5 Completed Date: - Revised Date: - |
Medline Journal Info:
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Nlm Unique ID: 9203577 Medline TA: Synlett Country: - |
Other Details:
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Languages: ENG Pagination: 667-674 Citation Subset: - |
Affiliation:
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Department of Chemistry, University of Pittsburgh, Pittsburgh, PA 15260, USA Fax +1(412)6249861. |
Export Citation:
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Descriptor/Qualifier:
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| Grant Support | |
ID/Acronym/Agency:
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R37 GM033372-26//NIGMS NIH HHS |
From MEDLINE®/PubMed®, a database of the U.S. National Library of Medicine
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