Document Detail


Extension of the liquid chromatography/quantitative structure-property relationship method to assess the lipophilicity of neutral, acidic, basic and amphotheric drugs.
MedLine Citation:
PMID:  22537604     Owner:  NLM     Status:  Publisher    
Abstract/OtherAbstract:
A reported chromatographic method to determine the 1-octanol/water partition coefficient (logP(o/w)) has been used to estimate the lipophilicity of 33 drugs with diverse structures and functionalities, including neutral, acid, basic, and amphoteric compounds. The applicability of the chromatographic method has been extended to the UHPLC technique, and the results obtained were compared to those obtained from conventional HPLC. No significant difference between the results obtained by both techniques is noticed. Thus, the suitability of UHPLC, which involves shorter run times, for lipophilicity assessment is demonstrated. In order to show the consistency of this chromatographic method, the logP(o/w) values of those drugs which have acid-base properties have been also determined by potentiometry, and the final results have been compared with both values derived from the chromatographic method and the ones from the literature.
Authors:
Juan M Pallicer; Carme Calvet; Adriana Port; Martí Rosés; Clara Ràfols; Elisabeth Bosch
Related Documents :
6174634 - Rapid semi-quantitative isolation of beta-2-microglobulin from urine.
22468814 - Mass spectrometry-based protein assays for in vitro diagnostic testing.
1695664 - Human chorionic gonadotrophin-like and beta-core-like materials in postmenopausal urine.
22475184 - Low crosslinking imprinted coatings based on liquid crystal for capillary electrochroma...
21355014 - Liquid chromatography-tandem mass spectrometry method for the measurement of serum meva...
19376664 - Isolation and characterization of a potential process related impurity of phenazopyridi...
Publication Detail:
Type:  JOURNAL ARTICLE     Date:  2012-4-5
Journal Detail:
Title:  Journal of chromatography. A     Volume:  -     ISSN:  1873-3778     ISO Abbreviation:  -     Publication Date:  2012 Apr 
Date Detail:
Created Date:  2012-4-27     Completed Date:  -     Revised Date:  -    
Medline Journal Info:
Nlm Unique ID:  9318488     Medline TA:  J Chromatogr A     Country:  -    
Other Details:
Languages:  ENG     Pagination:  -     Citation Subset:  -    
Copyright Information:
Copyright © 2012 Elsevier B.V. All rights reserved.
Affiliation:
Departament de Química Analítica and Institut de Biomedicina (IBUB), Universitat de Barcelona, Martí i Franquès 1-11, 08028 Barcelona, Spain.
Export Citation:
APA/MLA Format     Download EndNote     Download BibTex
MeSH Terms
Descriptor/Qualifier:

From MEDLINE®/PubMed®, a database of the U.S. National Library of Medicine


Previous Document:  Short and long terms healing of the experimentally transverse sectioned tendon in rabbits.
Next Document:  Untargeted screening of urinary peptides with liquid chromatography coupled to hybrid linear-ion tra...