Document Detail


Experimental artefacts in 2D-MAS exchange experiments: non-uniform mixing time within a single 2D run.
MedLine Citation:
PMID:  9694395     Owner:  NLM     Status:  MEDLINE    
Abstract/OtherAbstract:
The practical realization of rotor-synchronized mixing-times in 2D-MAS exchange experiments without the need for a special hardware is reviewed; its consequence for the 'true mixing time' of the experiment is discussed. We demonstrate influences on experimental rate constants derived from such experiments as well as on the appearance of the 2D-MAS spectra, taken at short mixing times.
Authors:
D Reichert; G Hempel; H Schneider
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Publication Detail:
Type:  Journal Article; Research Support, Non-U.S. Gov't    
Journal Detail:
Title:  Solid state nuclear magnetic resonance     Volume:  11     ISSN:  0926-2040     ISO Abbreviation:  Solid State Nucl Magn Reson     Publication Date:  1998 Jun 
Date Detail:
Created Date:  1998-10-06     Completed Date:  1998-10-06     Revised Date:  2006-11-15    
Medline Journal Info:
Nlm Unique ID:  9306181     Medline TA:  Solid State Nucl Magn Reson     Country:  NETHERLANDS    
Other Details:
Languages:  eng     Pagination:  259-64     Citation Subset:  IM    
Affiliation:
Univ. of Halle, Dept. of Physics, Germany. reichert@physik.uni-halle.de
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MeSH Terms
Descriptor/Qualifier:
Artifacts*
Humans
Magnetic Resonance Spectroscopy / diagnostic use,  methods*

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