Document Detail


Enantioresolution of fluorinated diphenylmethanols and determination of their absolute configurations by X-Ray crystallographic and 1H NMR anisotropy methods.
MedLine Citation:
PMID:  14628296     Owner:  NLM     Status:  PubMed-not-MEDLINE    
Abstract/OtherAbstract:
Various fluorinated diphenylmethanols were enantioresolved by the methods of chiral camphorsultam-dichlorophthalic acid (CSDP acid) and/or 2-methoxy-2-(1-naphthyl)propionic acid (MalphaNP acid) yielding enantiopure alcohols. Their absolute configurations were unambiguously determined by X-ray crystallography of CSDP esters and/or by the (1)H NMR anisotropy method of MalphaNP esters for the first time.
Authors:
Junpei Naito; Masashi Kosaka; Takeo Sugito; Masataka Watanabe; Nobuyuki Harada; William H Pirkle
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Publication Detail:
Type:  Journal Article    
Journal Detail:
Title:  Chirality     Volume:  16     ISSN:  0899-0042     ISO Abbreviation:  Chirality     Publication Date:  2004 Jan 
Date Detail:
Created Date:  2003-11-20     Completed Date:  2004-02-09     Revised Date:  -    
Medline Journal Info:
Nlm Unique ID:  8914261     Medline TA:  Chirality     Country:  United States    
Other Details:
Languages:  eng     Pagination:  22-35     Citation Subset:  -    
Copyright Information:
Copyright 2003 Wiley-Liss, Inc.
Affiliation:
Institute of Multidisciplinary Research for Advanced Materials, Tohoku University, Sendai, Japan.
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