Document Detail


Effect of surface acidity and basicity of aluminas on asphaltene adsorption and oxidation.
MedLine Citation:
PMID:  21571295     Owner:  NLM     Status:  Publisher    
Abstract/OtherAbstract:
This study investigates the effect of surface acidity and basicity of aluminas on asphaltene adsorption followed by air oxidation. Equilibrium batch adsorption experiments were conducted at 25°C with solutions of asphaltenes in toluene at concentrations ranging from 100 to 3000g/L using three conventional alumina adsorbents with different surface acidity. Data were found to better fit to the Freundlich isotherm model showing a multilayer adsorption. Results showed that asphaltene adsorption is strongly affected by the surface acidity, and the adsorption capacities of asphaltenes onto the three aluminas followed the order acidic>basic and neutral. Asphaltenes adsorbed over aluminas were subjected to oxidation in air up to 600°C in a thermogravimetric analyzer to study the catalytic effect of aluminas with different surface acidity. A correlation was found between Freundlich affinity constant (1/n) and the catalytic activity. Basic alumina that has the lowest 1/n value, depicting strongest interactions, has the highest catalytic activity, followed by neutral and acidic aluminas, respectively.
Authors:
Nashaat N Nassar; Azfar Hassan; Pedro Pereira-Almao
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Publication Detail:
Type:  JOURNAL ARTICLE     Date:  2011-4-27
Journal Detail:
Title:  Journal of colloid and interface science     Volume:  -     ISSN:  1095-7103     ISO Abbreviation:  -     Publication Date:  2011 Apr 
Date Detail:
Created Date:  2011-5-16     Completed Date:  -     Revised Date:  -    
Medline Journal Info:
Nlm Unique ID:  0043125     Medline TA:  J Colloid Interface Sci     Country:  -    
Other Details:
Languages:  ENG     Pagination:  -     Citation Subset:  -    
Copyright Information:
Copyright © 2011 Elsevier Inc. All rights reserved.
Affiliation:
Department of Chemical & Petroleum Engineering, Alberta Ingenuity Centre for In-Situ Energy, University of Calgary, Calgary, Alberta, Canada.
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