Document Detail

(E)-4-(2-Chloro-benzyl-ideneamino)-3-(2-chloro-phen-yl)-1H-1,2,4-triazole-5(4H)-thione-(E)-1,5-bis-(2-chloro-benzyl-idene)thio-carbonohydrazide-methanol (1/1/1).
MedLine Citation:
PMID:  21580033     Owner:  NLM     Status:  PubMed-not-MEDLINE    
In the title compound, C(15)H(12)Cl(2)N(4)S·C(15)H(10)Cl(2)N(4)S·C(2)H(6)O, the two chloro-phenyl rings of the triazole derivative form dihedral angles of 65.7 (2) and 44.2 (2)° with the triazole ring. In the thio-carbonohydrazide derivative, the dihedral angle between the two chloro-phenyl rings is 5.4 (2)°. In the crystal, the triazole, thio-carbonohydrazide and methanol mol-ecules are linked by N-H⋯O, N-H⋯S and O-H⋯S hydrogen bonds, forming a hexa-meric unit.
Qingliang Guo
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Publication Detail:
Type:  Journal Article     Date:  2009-12-16
Journal Detail:
Title:  Acta crystallographica. Section E, Structure reports online     Volume:  66     ISSN:  1600-5368     ISO Abbreviation:  Acta Crystallogr E Struct Rep Online     Publication Date:  2009  
Date Detail:
Created Date:  2011-05-17     Completed Date:  2011-07-14     Revised Date:  2011-11-11    
Medline Journal Info:
Nlm Unique ID:  101089178     Medline TA:  Acta Crystallogr E Struct Rep Online     Country:  England    
Other Details:
Languages:  eng     Pagination:  o141     Citation Subset:  -    
Department of Chemistry and Environmental Science, Taishan University, 271021 Taian, Shandong, People's Republic of China.
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