Document Detail


Dimethyl titanocene Y: a valuable precursor for libraries of cytotoxic titanocene derivatives.
MedLine Citation:
PMID:  20452674     Owner:  NLM     Status:  MEDLINE    
Abstract/OtherAbstract:
Reaction of the known titanocene Y 2 with methyl lithium at -15 degrees C yields bis-[(p-methoxybenzyl)cyclopentadienyl]titanium(IV) dimethyl (dimethyl titanocene Y, 3), a hitherto unknown, surprisingly robust titanium (IV) dimethyl species. Dimethyl titanocene Y was utilized in the preparation of several bis-[(p-methoxybenzyl)cyclopentadienyl]titanium(IV) dicarboxylates by the reaction with the free carboxylic acids in fair to good yields. Cytotoxicity of all new compounds has been estimated in Hela S3 cells.
Authors:
Timo A Immel; Josefine T Martin; Christoph J Dürr; Ulrich Groth; Thomas Huhn
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Publication Detail:
Type:  Journal Article; Research Support, Non-U.S. Gov't     Date:  2010-04-24
Journal Detail:
Title:  Journal of inorganic biochemistry     Volume:  104     ISSN:  1873-3344     ISO Abbreviation:  J. Inorg. Biochem.     Publication Date:  2010 Aug 
Date Detail:
Created Date:  2010-06-11     Completed Date:  2010-09-10     Revised Date:  -    
Medline Journal Info:
Nlm Unique ID:  7905788     Medline TA:  J Inorg Biochem     Country:  United States    
Other Details:
Languages:  eng     Pagination:  863-7     Citation Subset:  IM    
Copyright Information:
(c) 2010 Elsevier Inc. All rights reserved.
Affiliation:
Fachbereich Chemie and Konstanz Research School Chemical Biology, Universität Konstanz, Universitätsstrasse 10, Fach 720, 78457 Konstanz, Germany.
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MeSH Terms
Descriptor/Qualifier:
Antibiotics, Antineoplastic* / chemical synthesis,  chemistry,  pharmacology
Drug Screening Assays, Antitumor / methods
Hela Cells
Humans
Organometallic Compounds* / chemical synthesis,  chemistry,  pharmacology
Chemical
Reg. No./Substance:
0/Antibiotics, Antineoplastic; 0/Organometallic Compounds; 0/dimethyl titanocene

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