Document Detail


Diaryl ether synthesis in supercritical carbon dioxide in batch and continuous flow modes.
MedLine Citation:
PMID:  18830491     Owner:  NLM     Status:  MEDLINE    
Abstract/OtherAbstract:
A high yielding, batch mode synthesis of diaryl ethers and sulfides by an S(N)Ar fluoride-mediated process in scCO(2) has been developed; the use of a polymer-supported imidazolium fluoride reagent in batch mode led to the development of a fixed-bed continuous flow process, with high conversions.
Authors:
Jin-Kyun Lee; Matthew J Fuchter; Rachel M Williamson; Gary A Leeke; Edward J Bush; Ian F McConvey; Simon Saubern; John H Ryan; Andrew B Holmes
Publication Detail:
Type:  Journal Article; Research Support, Non-U.S. Gov't     Date:  2008-08-06
Journal Detail:
Title:  Chemical communications (Cambridge, England)     Volume:  -     ISSN:  1359-7345     ISO Abbreviation:  Chem. Commun. (Camb.)     Publication Date:  2008 Oct 
Date Detail:
Created Date:  2008-10-02     Completed Date:  2008-12-16     Revised Date:  -    
Medline Journal Info:
Nlm Unique ID:  9610838     Medline TA:  Chem Commun (Camb)     Country:  England    
Other Details:
Languages:  eng     Pagination:  4780-2     Citation Subset:  IM    
Affiliation:
Department of Chemistry, University of Cambridge, Cambridge, UK CB2 1EW.
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MeSH Terms
Descriptor/Qualifier:
Carbon Dioxide / chemistry*
Chromatography, High Pressure Liquid / methods
Chromatography, Supercritical Fluid
Ethers / chemical synthesis*,  chemistry
Fluorobenzenes / chemistry
Molecular Structure
Pressure
Sulfides / chemical synthesis,  chemistry
Chemical
Reg. No./Substance:
0/Ethers; 0/Fluorobenzenes; 0/Sulfides; 124-38-9/Carbon Dioxide

From MEDLINE®/PubMed®, a database of the U.S. National Library of Medicine


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