Document Detail


Determination of uric acid by an anion-exchange column chromatography.
MedLine Citation:
PMID:  3619024     Owner:  NLM     Status:  MEDLINE    
Abstract/OtherAbstract:
A column chromatography using a conventional anion-exchange resin for the separation of uric acid from other purine metabolites is described. It uses a HCl gradient, and the amount of uric acid is quantified directly by monitoring the absorbance of the effluent at 285 nm. The linear range of response is 0.5 to 100 nmol. The method was applied to the analysis of uric acid in urine and serum. Urine was injected directly into the system, while serum required removal of an interfering substance which absorbs the light and coelutes with uric acid. However, this substance was simply removed by heat coagulation of serum by heating in a boiling water bath for 2 min.
Authors:
D S Hsu; S S Chen
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Publication Detail:
Type:  Journal Article    
Journal Detail:
Title:  Analytical biochemistry     Volume:  163     ISSN:  0003-2697     ISO Abbreviation:  Anal. Biochem.     Publication Date:  1987 May 
Date Detail:
Created Date:  1987-08-31     Completed Date:  1987-08-31     Revised Date:  2008-11-21    
Medline Journal Info:
Nlm Unique ID:  0370535     Medline TA:  Anal Biochem     Country:  UNITED STATES    
Other Details:
Languages:  eng     Pagination:  238-41     Citation Subset:  IM    
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MeSH Terms
Descriptor/Qualifier:
Anion Exchange Resins
Chromatography, Ion Exchange
Hot Temperature
Humans
Urate Oxidase
Uric Acid / analysis*,  blood,  urine
Chemical
Reg. No./Substance:
0/Anion Exchange Resins; 69-93-2/Uric Acid; EC 1.7.3.3/Urate Oxidase

From MEDLINE®/PubMed®, a database of the U.S. National Library of Medicine


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