Document Detail


Determination of acetylsalicylic acid and metabolites in biological fluids by high-performance liquid chromatography.
MedLine Citation:
PMID:  6833429     Owner:  NLM     Status:  MEDLINE    
Abstract/OtherAbstract:
A new method has been developed for the determination of acetylsalicylic acid, salicylic acid, salicyluric acid and gentisic acid in plasma, urine and tissue homogenates by simple extraction with ethyl acetate, evaporation and redissolution and measuring by high-performance liquid chromatography. Linearity, reproducibility and recovery were determined. Experiments were carried out to investigate the decomposition of acetylsalicylic acid in plasma with fluoride at different temperatures. The method has been used for pharmacokinetic experiments and an example is given.
Authors:
U Reidl
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Publication Detail:
Type:  Journal Article    
Journal Detail:
Title:  Journal of chromatography     Volume:  272     ISSN:  0021-9673     ISO Abbreviation:  J. Chromatogr.     Publication Date:  1983 Feb 
Date Detail:
Created Date:  1983-05-27     Completed Date:  1983-05-27     Revised Date:  2004-11-17    
Medline Journal Info:
Nlm Unique ID:  0427043     Medline TA:  J Chromatogr     Country:  NETHERLANDS    
Other Details:
Languages:  eng     Pagination:  325-31     Citation Subset:  IM    
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MeSH Terms
Descriptor/Qualifier:
Animals
Aspirin / analysis,  metabolism*
Chromatography, High Pressure Liquid / methods
Gentisates / analysis
Hippurates / analysis
Humans
Kinetics
Male
Rabbits
Salicylic Acid
Salicylic Acids / analysis
Specimen Handling
Chemical
Reg. No./Substance:
0/Gentisates; 0/Hippurates; 0/Salicylic Acids; 487-54-7/salicylurate; 50-78-2/Aspirin; 69-72-7/Salicylic Acid

From MEDLINE®/PubMed®, a database of the U.S. National Library of Medicine


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